C₁₉H₂₇NO₅

Base Information

Chemical Name:C₁₉H₂₇NO₅
CAS No.:1408058-34-3
Molecular Formula:C₁₉H₂₇NO₅
Molecular Weight:349.427
Hs Code.:

C<sub>19</sub>H<sub>27</sub>NO<sub>5</sub>

Synonyms:C₁₉H₂₇NO₅

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Chemical Property of C₁₉H₂₇NO₅

Chemical Property:

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Technology Process of C₁₉H₂₇NO₅

There total 15 articles about C₁₉H₂₇NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1408058-32-1
C₁₉H₂₉NO₅

: 1408058-34-3
C₁₉H₂₇NO₅

Guidance literature:: C₁₉H₂₉NO₅; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 1h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - 20 ℃; for 0.75h; Inert atmosphere;
DOI:org/10.1016/j.tetlet.2012.08.143

Reference yield:

: 1393086-00-4
C₁₇H₂₂O₅

: 1408058-34-3
C₁₉H₂₇NO₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium tetrahydroborate / ethanol / 2 h / 20 °C

2.1: pyridine / dichloromethane / 2 h / 20 °C

3.1: copper(II) bis(trifluoromethanesulfonate); borane-THF / 0.17 h / 20 °C / Inert atmosphere

4.1: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C / Inert atmosphere

5.1: pyridine / dichloromethane / 1 h / -15 °C / Inert atmosphere

6.1: sodium azide / N,N-dimethyl-formamide / 2 h / 20 °C

7.1: triphenylphosphine / tetrahydrofuran / 4 h / 20 °C

7.2: 4 h / 20 °C

8.1: pyridine / 2 h / 0 - 20 °C

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

10.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 1 h / -78 °C / Inert atmosphere

10.2: 0.75 h / -78 - 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; dmap; sodium tetrahydroborate; sodium azide; borane-THF; oxalyl dichloride; tetrabutyl ammonium fluoride; copper(II) bis(trifluoromethanesulfonate); dimethyl sulfoxide; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; 7.1: |Staudinger Azide Reduction / 7.2: |Staudinger Azide Reduction / 10.1: |Swern Oxidation / 10.2: |Swern Oxidation;
DOI:org/10.1016/j.tetlet.2012.08.143

Reference yield:

: 3458-28-4
D-Mannose

: 1408058-34-3
C₁₉H₂₇NO₅

Guidance literature:: Multi-step reaction with 12 steps

1.1: sulfuric acid / N,N-dimethyl-formamide / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide

2.2: 4 h / 20 °C

3.1: hydrogenchloride; water / methanol / 4 h / 20 °C

4.1: sodium periodate / ethanol; water; methanol / 3 h / 20 °C

5.1: copper(II) bis(trifluoromethanesulfonate); borane-THF / 2 h / 20 °C / Inert atmosphere

6.1: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C / Inert atmosphere

7.1: pyridine / dichloromethane / 1 h / -15 °C / Inert atmosphere

8.1: sodium azide / N,N-dimethyl-formamide / 2 h / 20 °C

9.1: triphenylphosphine / tetrahydrofuran / 4 h / 20 °C

9.2: 4 h / 20 °C

10.1: pyridine / 2 h / 0 - 20 °C

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

12.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 1 h / -78 °C / Inert atmosphere

12.2: 0.75 h / -78 - 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; hydrogenchloride; dmap; sodium periodate; sodium azide; borane-THF; oxalyl dichloride; sulfuric acid; tetrabutyl ammonium fluoride; water; copper(II) bis(trifluoromethanesulfonate); sodium hydride; dimethyl sulfoxide; triphenylphosphine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; 9.1: |Staudinger Azide Reduction / 9.2: |Staudinger Azide Reduction / 12.1: |Swern Oxidation / 12.2: |Swern Oxidation;
DOI:org/10.1016/j.tetlet.2012.08.143