1-<2-hydroxy-4,6-bis(methoxymethoxy)-3-methylphenyl>-3-(4-methoxyphenyl)-2-propen-1-on

Base Information

• Chemical Name: 1-<2-hydroxy-4,6-bis(methoxymethoxy)-3-methylphenyl>-3-(4-methoxyphenyl)-2-propen-1-on
• CAS No.: 106929-63-9
• Molecular Formula: C₂₁H₂₄O₇
• Molecular Weight: 388.417

Synonyms:1-<2-hydroxy-4,6-bis(methoxymethoxy)-3-methylphenyl>-3-(4-methoxyphenyl)-2-propen-1-on

Chemical Property of 1-<2-hydroxy-4,6-bis(methoxymethoxy)-3-methylphenyl>-3-(4-methoxyphenyl)-2-propen-1-on

Chemical Property:

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Technology Process of 1-<2-hydroxy-4,6-bis(methoxymethoxy)-3-methylphenyl>-3-(4-methoxyphenyl)-2-propen-1-on

There total 2 articles about 1-<2-hydroxy-4,6-bis(methoxymethoxy)-3-methylphenyl>-3-(4-methoxyphenyl)-2-propen-1-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4,6-trihydroxy-3-methyl-acetophenon (2657-28-5) → 1-<2-hydroxy-4,6-bis(methoxymethoxy)-3-methylphenyl>-3-(4-methoxyphenyl)-2-propen-1-on (106929-63-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 34 percent / K₂CO₃ / acetone / 1 h / 0 °C

2: 1) piperidine; 2) 0.25 N NaOEt / 1) 72 h, heating; 2) heating

With piperidine; sodium ethanolate; potassium carbonate; In acetone;

Reference yield:

4-methoxy-benzaldehyde (123-11-5) + 3-methyl-2-hydroxy-4,6-bis(methoxymethoxy)acetophenone (106929-57-1) → 1-<2-hydroxy-4,6-bis(methoxymethoxy)-3-methylphenyl>-3-(4-methoxyphenyl)-2-propen-1-on (106929-63-9)

Guidance literature:

With piperidine; sodium ethanolate; Yield given. Multistep reaction; 1) 72 h, heating; 2) heating;

Reference yield: 57.0%

1-<2-hydroxy-4,6-bis(methoxymethoxy)-3-methylphenyl>-3-(4-methoxyphenyl)-2-propen-1-on (106929-63-9) → 1-<2-hydroxy-4,6-bis(methoxymethoxy)-3-methylphenyl>-3-(4-methoxyphenyl)-propan-1-on (106946-99-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetone;

upstream raw materials:

4-methoxy-benzaldehyde

3-methyl-2-hydroxy-4,6-bis(methoxymethoxy)acetophenone

2,4,6-trihydroxy-3-methyl-acetophenon

Downstream raw materials:

1-<2-hydroxy-4,6-bis(methoxymethoxy)-3-methylphenyl>-3-(4-methoxyphenyl)-propan-1-on

5,7-dihydroxy-3-(4-methoxybenzyl)-6-methylchromone

5,7-dihydroxy-3-(4-methoxybenzyl)-8-methyl-4H-1-benzopyran-4-on

1-(2-benzyloxy-4,6-dihydroxy-3-methylphenyl)-3-(4-methoxyphenyl)propan-1-on

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