N,N-diethyl 3,6-dideoxy-3,6-imino-N'-benzyl-4,5-O-isopropylidene-7-O-trityl-L-glycero-D-manno-heptonamide

Base Information

Chemical Name:N,N-diethyl 3,6-dideoxy-3,6-imino-N'-benzyl-4,5-O-isopropylidene-7-O-trityl-L-glycero-D-manno-heptonamide
CAS No.:688321-38-2
Molecular Formula:C₄₀H₄₆N₂O₅
Molecular Weight:634.816
Hs Code.:

Synonyms:N,N-diethyl 3,6-dideoxy-3,6-imino-N'-benzyl-4,5-O-isopropylidene-7-O-trityl-L-glycero-D-manno-heptonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-diethyl 3,6-dideoxy-3,6-imino-N'-benzyl-4,5-O-isopropylidene-7-O-trityl-L-glycero-D-manno-heptonamide

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Technology Process of N,N-diethyl 3,6-dideoxy-3,6-imino-N'-benzyl-4,5-O-isopropylidene-7-O-trityl-L-glycero-D-manno-heptonamide

There total 4 articles about N,N-diethyl 3,6-dideoxy-3,6-imino-N'-benzyl-4,5-O-isopropylidene-7-O-trityl-L-glycero-D-manno-heptonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 100-46-9
benzylamine

: 688321-37-1
N,N-diethyl 2,3-anhydro-4,5-O-isopropylidene-7-O-trityl-D-altro-6-heptulosamide

: N,N-diethyl-2-hydroxy-2-(6-hydroxy-2,2-dimethyl-6-trityloxymethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-acetamide

: 688321-38-2
N,N-diethyl 3,6-dideoxy-3,6-imino-N'-benzyl-4,5-O-isopropylidene-7-O-trityl-L-glycero-D-manno-heptonamide

Guidance literature:: With sodium cyanoborohydride; zinc(II) chloride; In ethanol; at 20 ℃; for 7h;
DOI:10.1016/j.tetasy.2004.11.054

Reference yield: 60.0%

: 100-46-9
benzylamine

: 688321-37-1
N,N-diethyl 2,3-anhydro-4,5-O-isopropylidene-7-O-trityl-D-altro-6-heptulosamide

: 688321-38-2
N,N-diethyl 3,6-dideoxy-3,6-imino-N'-benzyl-4,5-O-isopropylidene-7-O-trityl-L-glycero-D-manno-heptonamide

Guidance literature:: benzylamine; N,N-diethyl 2,3-anhydro-4,5-O-isopropylidene-7-O-trityl-D-altro-6-heptulosamide; With zinc(II) chloride;

With sodium cyanoborohydride; In ethanol; for 7h; Further stages.;
DOI:10.1016/j.tetlet.2004.01.144