Toluene-4-sulfonate(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-pentafluorophenyl-iodonium;

Base Information

Chemical Name:Toluene-4-sulfonate(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-pentafluorophenyl-iodonium;
CAS No.:111873-56-4
Molecular Formula:C₇H₇O₃S*C₁₄H₁₁F₅IO₂
Molecular Weight:604.333
Hs Code.:

Synonyms:Toluene-4-sulfonate(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-pentafluorophenyl-iodonium;

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Chemical Property of Toluene-4-sulfonate(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-pentafluorophenyl-iodonium;

Chemical Property:

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Technology Process of Toluene-4-sulfonate(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-pentafluorophenyl-iodonium;

There total 3 articles about Toluene-4-sulfonate(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-pentafluorophenyl-iodonium; which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 126-81-8
dimedone

: 111873-52-0
(hydroxy(tosyloxy)iodo)pentafluorobenzene

: 111873-56-4
Toluene-4-sulfonate(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-pentafluorophenyl-iodonium;

Guidance literature:: In chloroform; for 0.25h; Ambient temperature;
DOI:10.1016/S0040-4039(01)81012-1

Reference yield:

: 14353-88-9
iodopentafluorobenzene bis(trifluoroacetate)

: 111873-56-4
Toluene-4-sulfonate(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-pentafluorophenyl-iodonium;

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / acetonitrile / 0.25 h / Ambient temperature

2: 90 percent / CHCl₃ / 0.25 h / Ambient temperature

In chloroform; acetonitrile;
DOI:10.1016/S0040-4039(01)81012-1

Reference yield:

: 104-15-4
toluene-4-sulfonic acid

: 111873-56-4
Toluene-4-sulfonate(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-pentafluorophenyl-iodonium;

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / acetonitrile / 0.25 h / Ambient temperature

2: 90 percent / CHCl₃ / 0.25 h / Ambient temperature

In chloroform; acetonitrile;
DOI:10.1016/S0040-4039(01)81012-1