Carbonic acid allyl ester 4-[(S)-2-allyloxycarbonylamino-2-(4-hydroxymethyl-phenylcarbamoyl)-ethyl]-phenyl ester

Base Information

• Chemical Name: Carbonic acid allyl ester 4-[(S)-2-allyloxycarbonylamino-2-(4-hydroxymethyl-phenylcarbamoyl)-ethyl]-phenyl ester
• CAS No.: 728916-20-9
• Molecular Formula: C₂₄H₂₆N₂O₇
• Molecular Weight: 454.48

Synonyms:Carbonic acid allyl ester 4-[(S)-2-allyloxycarbonylamino-2-(4-hydroxymethyl-phenylcarbamoyl)-ethyl]-phenyl ester

Chemical Property of Carbonic acid allyl ester 4-[(S)-2-allyloxycarbonylamino-2-(4-hydroxymethyl-phenylcarbamoyl)-ethyl]-phenyl ester

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of Carbonic acid allyl ester 4-[(S)-2-allyloxycarbonylamino-2-(4-hydroxymethyl-phenylcarbamoyl)-ethyl]-phenyl ester

There total 1 articles about Carbonic acid allyl ester 4-[(S)-2-allyloxycarbonylamino-2-(4-hydroxymethyl-phenylcarbamoyl)-ethyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

4-aminobenzenemethanol (623-04-1) + N,O-bis-allyloxycarbonyl-L-tyrosine (104669-68-3) → Carbonic acid allyl ester 4-[(S)-2-allyloxycarbonylamino-2-(4-hydroxymethyl-phenylcarbamoyl)-ethyl]-phenyl ester (728916-20-9)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1016/j.bmc.2005.08.015

Reference yield: 99.0%

4-Nitrophenyl chloroformate (7693-46-1) + Carbonic acid allyl ester 4-[(S)-2-allyloxycarbonylamino-2-(4-hydroxymethyl-phenylcarbamoyl)-ethyl]-phenyl ester (728916-20-9) → C31H29N3O11 (875153-71-2)

Guidance literature:

With pyridine; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.bmcl.2004.04.041

Reference yield: 98.0%

7-isocyanato-4-methylcoumarine + Carbonic acid allyl ester 4-[(S)-2-allyloxycarbonylamino-2-(4-hydroxymethyl-phenylcarbamoyl)-ethyl]-phenyl ester (728916-20-9) → carbonic acid allyl ester 4-{2-allyloxycarbonylamino-2-[4-(4-methyl-2-oxo-2H-chromen-7-ylcarbamoyloxymethyl)-phenylcarbamoyl]-ethyl}-phenyl ester (728916-21-0)

Guidance literature:

In toluene; for 2h; Heating;

DOI:10.1016/j.bmcl.2004.04.041 DOI:10.1016/j.bmc.2005.08.015

upstream raw materials:

4-aminobenzenemethanol

N,O-bis-allyloxycarbonyl-L-tyrosine

Downstream raw materials:

C₃₁H₂₉N₃O₁₁

carbonic acid allyl ester 4-{2-allyloxycarbonylamino-2-[4-(4-methyl-2-oxo-2H-chromen-7-ylcarbamoyloxymethyl)-phenylcarbamoyl]-ethyl}-phenyl ester

Carbonic acid allyl ester 4-{(S)-2-allyloxycarbonylamino-2-[4-(2-methyl-9,10-dioxo-9,10-dihydro-anthracen-1-ylcarbamoyloxymethyl)-phenylcarbamoyl]-ethyl}-phenyl ester

(4-methyl-2-oxo-2H-chromen-7-yl)-carbamic acid 4-[2-amino-3-(4-hydroxy-phenyl)-propionylamino]-benzyl ester

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