<2S-(2α(7R^*,8R^*),3aα,4β,7β,7aα)>-2-Methyl-8-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>octadecan-7-ol,4-methylbenzolsulfonat

Base Information

• Chemical Name: <2S-(2α(7R^*,8R^*),3aα,4β,7β,7aα)>-2-Methyl-8-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>octadecan-7-ol,4-methylbenzolsulfonat
• CAS No.: 130209-64-2
• Molecular Formula: C₃₈H₆₄O₅S
• Molecular Weight: 632.989

Synonyms:<2S-(2α(7R^*,8R^*),3aα,4β,7β,7aα)>-2-Methyl-8-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>octadecan-7-ol,4-methylbenzolsulfonat

Chemical Property of <2S-(2α(7R^*,8R^*),3aα,4β,7β,7aα)>-2-Methyl-8-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>octadecan-7-ol,4-methylbenzolsulfonat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of <2S-(2α(7R^*,8R^*),3aα,4β,7β,7aα)>-2-Methyl-8-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>octadecan-7-ol,4-methylbenzolsulfonat

There total 1 articles about <2S-(2α(7R^*,8R^*),3aα,4β,7β,7aα)>-2-Methyl-8-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>octadecan-7-ol,4-methylbenzolsulfonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

<2S-(2α(7R*,8R*),3aα,4β,7β,7aα)>-2-Methyl-8-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>octadecan-7-ol (132881-30-2) + p-toluenesulfonyl chloride (98-59-9) → <2S-(2α(7R*,8R*),3aα,4β,7β,7aα)>-2-Methyl-8-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>octadecan-7-ol,4-methylbenzolsulfonat (130209-64-2)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1) pyridine, 30 deg C, 15 min, 2) r.t, 15h;

DOI:10.1007/BF00815171

Reference yield: 97.0%

glycolic Acid (79-14-1) + <2S-(2α(7R*,8R*),3aα,4β,7β,7aα)>-2-Methyl-8-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>octadecan-7-ol,4-methylbenzolsulfonat (130209-64-2) → *,R*)>-2-Methyl-7,8-octadecandiol,7-(4-methyl-benzolsulfonat) (54848-41-8) + <2S-(2α,3aα,4β,7β,7aα)>--essigsaeure (134020-80-7)

Guidance literature:

With toluene-4-sulfonic acid; In tetrahydrofuran; for 3h; Ambient temperature;

DOI:10.1007/BF00815171

Reference yield: 85.0%

<2S-(2α(7R*,8R*),3aα,4β,7β,7aα)>-2-Methyl-8-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>octadecan-7-ol,4-methylbenzolsulfonat (130209-64-2) → *,R*)>-2-Methyl-7,8-octadecandiol,7-(4-methyl-benzolsulfonat) (54848-41-8) + <2S-(2α,3aα,4β,7β,7aα)>--essigsaeure (134020-80-7)

Guidance literature:

With glycolic Acid; toluene-4-sulfonic acid; In tetrahydrofuran; for 3h; Ambient temperature;

DOI:10.1007/BF00815171

upstream raw materials:

<2S-(2α(7R^*,8R^*),3aα,4β,7β,7aα)>-2-Methyl-8-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>octadecan-7-ol

p-toluenesulfonyl chloride

Downstream raw materials:

*,R^*)>-2-Methyl-7,8-octadecandiol,7-(4-methyl-benzolsulfonat)

<2S-(2α,3aα,4β,7β,7aα)>--essigsaeure

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