(S)-2-Methyl-pentanoic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Base Information

Chemical Name:(S)-2-Methyl-pentanoic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester
CAS No.:122778-51-2
Molecular Formula:C₁₆H₃₀O₂
Molecular Weight:254.413
Hs Code.:

Synonyms:(S)-2-Methyl-pentanoic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-Methyl-pentanoic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

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Technology Process of (S)-2-Methyl-pentanoic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

There total 5 articles about (S)-2-Methyl-pentanoic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 122778-50-1
(S)-2-Chloromethyl-pentanoic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: 122778-51-2
(S)-2-Methyl-pentanoic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 10h; Heating;

Reference yield:

: 2216-51-5
(-)-menthol

: 122778-51-2
(S)-2-Methyl-pentanoic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 63 percent / dicyclohexylcarbodi-imide, 4-(N,N-dimethylamino)pyridine / acetonitrile; CH₂Cl₂ / -40 deg C, 6 h; room temperature, 10 h

2: 1.) oxalyl chloride, 2.) tetrabutylammonium borohydride / 1.) CH₂Cl₂, reflux, 2 h, 2.) -78 deg C, 30 min

3: 76.5 percent / Ph₃P, CCl₄ / 15 h / Heating

4: 95 percent / tributyltin hydride, AIBN / benzene / 10 h / Heating

With tetrachloromethane; dmap; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; tetrabutylammonium borohydride; dicyclohexyl-carbodiimide; triphenylphosphine; In dichloromethane; acetonitrile; benzene;

Reference yield:

: 122778-23-8,122778-24-9
(1R,3R,4S)-p-menthan-3-yl hydrogen propylmalonate

: 122778-51-2
(S)-2-Methyl-pentanoic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) oxalyl chloride, 2.) tetrabutylammonium borohydride / 1.) CH₂Cl₂, reflux, 2 h, 2.) -78 deg C, 30 min

2: 76.5 percent / Ph₃P, CCl₄ / 15 h / Heating

3: 95 percent / tributyltin hydride, AIBN / benzene / 10 h / Heating

With tetrachloromethane; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; tetrabutylammonium borohydride; triphenylphosphine; In benzene;