3-ethylenedioxy-1,2,3,4,6,7,8,8a-octahydro-8a-phenylmethylnaphthalene

Base Information

Chemical Name:3-ethylenedioxy-1,2,3,4,6,7,8,8a-octahydro-8a-phenylmethylnaphthalene
CAS No.:82911-92-0
Molecular Formula:C₁₉H₂₄O₂
Molecular Weight:284.398
Hs Code.:

Synonyms:3-ethylenedioxy-1,2,3,4,6,7,8,8a-octahydro-8a-phenylmethylnaphthalene

Suppliers and Price of 3-ethylenedioxy-1,2,3,4,6,7,8,8a-octahydro-8a-phenylmethylnaphthalene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-ethylenedioxy-1,2,3,4,6,7,8,8a-octahydro-8a-phenylmethylnaphthalene

Chemical Property:

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Technology Process of 3-ethylenedioxy-1,2,3,4,6,7,8,8a-octahydro-8a-phenylmethylnaphthalene

There total 3 articles about 3-ethylenedioxy-1,2,3,4,6,7,8,8a-octahydro-8a-phenylmethylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 107-21-1
ethylene glycol

: 70043-58-2
1,2,3,5,6,7,8,8a-octahydro-3-oxo-8a-phenylmethylnaphthalene

: 82911-92-0
3-ethylenedioxy-1,2,3,4,6,7,8,8a-octahydro-8a-phenylmethylnaphthalene

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 18h; Heating;
DOI:10.1139/v82-151

Reference yield:

: 946-33-8
2-benzylcyclohexan-1-one

: 82911-92-0
3-ethylenedioxy-1,2,3,4,6,7,8,8a-octahydro-8a-phenylmethylnaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / potassium hydroxide / diethyl ether; ethanol / 4 h / 0 °C

2: 77 percent / p-toluenesulfonic acid monohydrate / benzene / 18 h / Heating

With potassium hydroxide; toluene-4-sulfonic acid; In diethyl ether; ethanol; benzene;
DOI:10.1139/v82-151

Reference yield:

: 100-44-7
benzyl chloride

: 82911-92-0
3-ethylenedioxy-1,2,3,4,6,7,8,8a-octahydro-8a-phenylmethylnaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / 1.) dioxane, reflux 16 h, 2.) dioxane, water, reflux, 2.5 h

2: 49 percent / potassium hydroxide / diethyl ether; ethanol / 4 h / 0 °C

3: 77 percent / p-toluenesulfonic acid monohydrate / benzene / 18 h / Heating

With potassium hydroxide; toluene-4-sulfonic acid; In diethyl ether; ethanol; benzene;
DOI:10.1139/v82-151