2-(tert-butyl-diphenyl-silanyloxymethyl)-5-methylsulfanyl-3,4-dihydro-2H-pyrrole

Base Information

Chemical Name:2-(tert-butyl-diphenyl-silanyloxymethyl)-5-methylsulfanyl-3,4-dihydro-2H-pyrrole
CAS No.:852674-75-0
Molecular Formula:C₂₂H₂₉NOSSi
Molecular Weight:383.63
Hs Code.:

2-(<i>tert</i>-butyl-diphenyl-silanyloxymethyl)-5-methylsulfanyl-3,4-dihydro-2<i>H</i>-pyrrole

Synonyms:2-(tert-butyl-diphenyl-silanyloxymethyl)-5-methylsulfanyl-3,4-dihydro-2H-pyrrole

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Chemical Property of 2-(tert-butyl-diphenyl-silanyloxymethyl)-5-methylsulfanyl-3,4-dihydro-2H-pyrrole

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Technology Process of 2-(tert-butyl-diphenyl-silanyloxymethyl)-5-methylsulfanyl-3,4-dihydro-2H-pyrrole

There total 4 articles about 2-(tert-butyl-diphenyl-silanyloxymethyl)-5-methylsulfanyl-3,4-dihydro-2H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 142890-13-9
(S)-5-[(tert-butyl)-diphenylsilyloxy-methyl]-2-thiopyrrolidinone

: 74-88-4
methyl iodide

: 852674-75-0
2-(tert-butyl-diphenyl-silanyloxymethyl)-5-methylsulfanyl-3,4-dihydro-2H-pyrrole

Guidance literature:: (S)-5-[(tert-butyl)-diphenylsilyloxy-methyl]-2-thiopyrrolidinone; methyl iodide; In dichloromethane; at 20 ℃; for 24h;

With sodium methylate; In methanol; dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/jo0501846

Reference yield:

: 17342-08-4
(S)-Pyroglutaminol

: 852674-75-0
2-(tert-butyl-diphenyl-silanyloxymethyl)-5-methylsulfanyl-3,4-dihydro-2H-pyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / 2 h / 20 °C

2: Lawesson's reagent / tetrahydrofuran / 2 h / 20 °C

3: CH₂Cl₂ / 5 h / 20 °C

With Lawessons reagent; 1H-imidazole; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2005.07.076

Reference yield:

: 132974-83-5
(5S)-5-[[(tert-butyldiphenylsilyl)oxy]methyl]pyrrolidin-2-one

: 852674-75-0
2-(tert-butyl-diphenyl-silanyloxymethyl)-5-methylsulfanyl-3,4-dihydro-2H-pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: Lawesson's reagent / tetrahydrofuran / 2 h / 20 °C

2: CH₂Cl₂ / 5 h / 20 °C

With Lawessons reagent; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2005.07.076