2,6-bis-(2-propoxy-3-(2-propoxy-5-aminobenzyl)-5-aminobenzyl)-4-aminophenyl propyl ether

Base Information

Chemical Name:2,6-bis-(2-propoxy-3-(2-propoxy-5-aminobenzyl)-5-aminobenzyl)-4-aminophenyl propyl ether
CAS No.:227001-52-7
Molecular Formula:C₄₉H₆₅N₅O₅
Molecular Weight:804.086
Hs Code.:

Synonyms:2,6-bis-(2-propoxy-3-(2-propoxy-5-aminobenzyl)-5-aminobenzyl)-4-aminophenyl propyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-bis-(2-propoxy-3-(2-propoxy-5-aminobenzyl)-5-aminobenzyl)-4-aminophenyl propyl ether

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Technology Process of 2,6-bis-(2-propoxy-3-(2-propoxy-5-aminobenzyl)-5-aminobenzyl)-4-aminophenyl propyl ether

There total 5 articles about 2,6-bis-(2-propoxy-3-(2-propoxy-5-aminobenzyl)-5-aminobenzyl)-4-aminophenyl propyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 227001-48-1
2,6-bis-(2-propoxy-3-(2-propoxy-5-nitrobenzyl)-5-nitrobenzyl)-4-nitrophenyl propyl ether

: 227001-52-7
2,6-bis-(2-propoxy-3-(2-propoxy-5-aminobenzyl)-5-aminobenzyl)-4-aminophenyl propyl ether

Guidance literature:: With hydrogen; nickel; In toluene; Ambient temperature;

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 227001-52-7
2,6-bis-(2-propoxy-3-(2-propoxy-5-aminobenzyl)-5-aminobenzyl)-4-aminophenyl propyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / ZnCl₂ / 120 - 130 °C

2: 58 percent / K₂CO₃ / acetone / 72 h / Ambient temperature

3: 91 percent / H₂ / Raney-Ni / toluene / Ambient temperature

With hydrogen; potassium carbonate; zinc(II) chloride; nickel; In acetone; toluene;

Reference yield:

: 59920-03-5
2,6-bis-(2-hydroxy-5-nitrobenzyl)-4-nitrophenol

: 227001-52-7
2,6-bis-(2-propoxy-3-(2-propoxy-5-aminobenzyl)-5-aminobenzyl)-4-aminophenyl propyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / ZnCO₃, HBr / acetic acid; acetic anhydride / 1) 70 deg C, 2) reflux

2: 80 percent / ZnCl₂ / 120 - 130 °C

3: 58 percent / K₂CO₃ / acetone / 72 h / Ambient temperature

4: 91 percent / H₂ / Raney-Ni / toluene / Ambient temperature

With hydrogen bromide; hydrogen; potassium carbonate; zinc(II) carbonate; zinc(II) chloride; nickel; In acetic anhydride; acetic acid; acetone; toluene;