2,6-bis-(2-propoxy-3-(2-propoxy-5-nitrobenzyl)-5-nitrobenzyl)-4-nitrophenyl propyl ether

Base Information

Chemical Name:2,6-bis-(2-propoxy-3-(2-propoxy-5-nitrobenzyl)-5-nitrobenzyl)-4-nitrophenyl propyl ether
CAS No.:227001-48-1
Molecular Formula:C₄₉H₅₅N₅O₁₅
Molecular Weight:954
Hs Code.:

Synonyms:2,6-bis-(2-propoxy-3-(2-propoxy-5-nitrobenzyl)-5-nitrobenzyl)-4-nitrophenyl propyl ether

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Chemical Property of 2,6-bis-(2-propoxy-3-(2-propoxy-5-nitrobenzyl)-5-nitrobenzyl)-4-nitrophenyl propyl ether

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Technology Process of 2,6-bis-(2-propoxy-3-(2-propoxy-5-nitrobenzyl)-5-nitrobenzyl)-4-nitrophenyl propyl ether

There total 4 articles about 2,6-bis-(2-propoxy-3-(2-propoxy-5-nitrobenzyl)-5-nitrobenzyl)-4-nitrophenyl propyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 106-94-5
propyl bromide

: 227001-43-6
2,6-bis-(2-hydroxy-3-(2-hydroxy-5-nitrobenzyl)-5-nitrobenzyl)-4-nitrophenol

: 227001-48-1
2,6-bis-(2-propoxy-3-(2-propoxy-5-nitrobenzyl)-5-nitrobenzyl)-4-nitrophenyl propyl ether

Guidance literature:: With potassium carbonate; In acetone; for 72h; Ambient temperature;

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 227001-48-1
2,6-bis-(2-propoxy-3-(2-propoxy-5-nitrobenzyl)-5-nitrobenzyl)-4-nitrophenyl propyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / ZnCl₂ / 120 - 130 °C

2: 58 percent / K₂CO₃ / acetone / 72 h / Ambient temperature

With potassium carbonate; zinc(II) chloride; In acetone;

Reference yield:

: 59920-03-5
2,6-bis-(2-hydroxy-5-nitrobenzyl)-4-nitrophenol

: 227001-48-1
2,6-bis-(2-propoxy-3-(2-propoxy-5-nitrobenzyl)-5-nitrobenzyl)-4-nitrophenyl propyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / ZnCO₃, HBr / acetic acid; acetic anhydride / 1) 70 deg C, 2) reflux

2: 80 percent / ZnCl₂ / 120 - 130 °C

3: 58 percent / K₂CO₃ / acetone / 72 h / Ambient temperature

With hydrogen bromide; potassium carbonate; zinc(II) carbonate; zinc(II) chloride; In acetic anhydride; acetic acid; acetone;