methyl 4,4'-difluorobenzilate

Base Information

• Chemical Name: methyl 4,4'-difluorobenzilate
• CAS No.: 207516-58-3
• Molecular Formula: C₁₅H₁₂F₂O₃
• Molecular Weight: 278.255
• Mol file: 207516-58-3.mol

Synonyms:methyl 4,4'-difluorobenzilate

Chemical Property of methyl 4,4'-difluorobenzilate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of methyl 4,4'-difluorobenzilate

There total 4 articles about methyl 4,4'-difluorobenzilate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

methyl iodide (74-88-4) → methyl 4,4'-difluorobenzilate (207516-58-3)

Guidance literature:

With ethanol; sodium;

4,4'-difluoro-benzilic acid; In ethanol; at 20 ℃; for 3h;

methyl iodide; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 24h;

Reference yield: 80.0%

C14H9F2O3(1-)*Na(1+) + methyl iodide (74-88-4) → methyl 4,4'-difluorobenzilate (207516-58-3)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 24h;

Reference yield:

4,4'-difluoro-benzilic acid (357-60-8) + methyl iodide (74-88-4) → methyl 4,4'-difluorobenzilate (207516-58-3)

Guidance literature:

With sodium; In ethanol; N,N-dimethyl-formamide;

upstream raw materials:

methanol

4,4'-difluoro-benzilic acid

methyl iodide