N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-mercapto acetamido)acetamide

Base Information

Chemical Name:N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-mercapto acetamido)acetamide
CAS No.:1393845-14-1
Molecular Formula:C₁₄H₁₇N₅O₂S
Molecular Weight:319.387
Hs Code.:

Synonyms:N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-mercapto acetamido)acetamide

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Chemical Property of N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-mercapto acetamido)acetamide

Chemical Property:

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Technology Process of N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-mercapto acetamido)acetamide

There total 3 articles about N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-mercapto acetamido)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1393845-20-9
N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-(tritylthio)acetamido)acetamide

: 1393845-14-1
N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-mercapto acetamido)acetamide

Guidance literature:: With chlorotriisopropylsilane; trifluoroacetic acid; In water; at 20 ℃; for 2h;
DOI:10.1039/c2ob25774b

Reference yield:

: 847490-49-7
tert-butyl (2-oxo-2-(prop-2-yn-1-ylamino)ethyl)carbamate

: 1393845-14-1
N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-mercapto acetamido)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 1.5 h / 0 °C

2: copper(ll) sulfate pentahydrate; sodium azide; sodium carbonate; sodium L-ascorbate; L-proline / water; dimethyl sulfoxide / 65 °C / Inert atmosphere

3: chlorotriisopropylsilane; trifluoroacetic acid / water / 2 h / 20 °C

With sodium azide; copper(ll) sulfate pentahydrate; chlorotriisopropylsilane; sodium carbonate; sodium L-ascorbate; trifluoroacetic acid; L-proline; In dichloromethane; water; dimethyl sulfoxide; 2: Huisgen 1,3-dipolar cyclization;
DOI:10.1039/c2ob25774b

Reference yield:

: 1393845-12-9
N-(2-oxo-2-(prop-2-yn-1-ylamino)ethyl)-2-(tritylthio)acetamide

: 1393845-14-1
N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-mercapto acetamido)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) sulfate pentahydrate; sodium azide; sodium carbonate; sodium L-ascorbate; L-proline / water; dimethyl sulfoxide / 65 °C / Inert atmosphere

2: chlorotriisopropylsilane; trifluoroacetic acid / water / 2 h / 20 °C

With sodium azide; copper(ll) sulfate pentahydrate; chlorotriisopropylsilane; sodium carbonate; sodium L-ascorbate; trifluoroacetic acid; L-proline; In water; dimethyl sulfoxide; 1: Huisgen 1,3-dipolar cyclization;
DOI:10.1039/c2ob25774b