N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-(tritylthio)acetamido)acetamide

Base Information

Chemical Name:N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-(tritylthio)acetamido)acetamide
CAS No.:1393845-20-9
Molecular Formula:C₃₃H₃₁N₅O₂S
Molecular Weight:561.707
Hs Code.:

Synonyms:N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-(tritylthio)acetamido)acetamide

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Chemical Property of N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-(tritylthio)acetamido)acetamide

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Technology Process of N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-(tritylthio)acetamido)acetamide

There total 4 articles about N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-(tritylthio)acetamido)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1393845-12-9
N-(2-oxo-2-(prop-2-yn-1-ylamino)ethyl)-2-(tritylthio)acetamide

: 100-39-0
benzyl bromide

: 1393845-20-9
N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-(tritylthio)acetamido)acetamide

Guidance literature:: With sodium azide; copper(ll) sulfate pentahydrate; sodium carbonate; sodium L-ascorbate; L-proline; In water; dimethyl sulfoxide; at 65 ℃; Inert atmosphere;
DOI:10.1039/c2ob25774b

Reference yield:

: 847490-49-7
tert-butyl (2-oxo-2-(prop-2-yn-1-ylamino)ethyl)carbamate

: 1393845-20-9
N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-(tritylthio)acetamido)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1.5 h / 0 °C

2: copper(ll) sulfate pentahydrate; sodium azide; sodium carbonate; sodium L-ascorbate; L-proline / water; dimethyl sulfoxide / 65 °C / Inert atmosphere

With sodium azide; copper(ll) sulfate pentahydrate; sodium carbonate; sodium L-ascorbate; trifluoroacetic acid; L-proline; In dichloromethane; water; dimethyl sulfoxide; 2: Huisgen 1,3-dipolar cyclization;
DOI:10.1039/c2ob25774b

Reference yield:

: 34914-36-8
2-(triphenylmethylthio)ethanoic acid

: 1393845-20-9
N-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-2-(2-(tritylthio)acetamido)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide / dichloromethane / 20 °C

2: copper(ll) sulfate pentahydrate; sodium azide; sodium carbonate; sodium L-ascorbate; L-proline / water; dimethyl sulfoxide / 65 °C / Inert atmosphere

With sodium azide; copper(ll) sulfate pentahydrate; sodium carbonate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; L-proline; In dichloromethane; water; dimethyl sulfoxide; 2: Huisgen 1,3-dipolar cyclization;
DOI:10.1039/c2ob25774b