C₁₈H₂₅NO₁₃

Base Information

• Chemical Name: C₁₈H₂₅NO₁₃
• CAS No.: 210832-21-6
• Molecular Formula: C₁₈H₂₅NO₁₃
• Molecular Weight: 463.395
• Mol file: 210832-21-6.mol

Synonyms:C₁₈H₂₅NO₁₃

Chemical Property of C₁₈H₂₅NO₁₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₂₅NO₁₃

There total 4 articles about C₁₈H₂₅NO₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

α-galactosyl fluoride (2021-84-3) + 4-nitrophenyl-α-D-glucopyranoside (3767-28-0) → C18H25NO13 (210832-21-6,335193-88-9)

Guidance literature:

With α-galactosidase from Bacteroides thetaiotaomicron D415G mutant; sodium formate; In aq. buffer; at 30 ℃; for 48h; pH=6; Reagent/catalyst; Enzymatic reaction;

DOI:10.1111/febs.14018

Reference yield:

1-amido-1-deoxygalactopyranose (35899-89-9) + 4-nitrophenyl-α-D-glucopyranoside (3767-28-0) → D-Galactose (10257-28-0) + C18H25NO13 (210832-21-6,335193-88-9)

Guidance literature:

With C-terminus histidine tagged α-galactosidase from Thermotoga maritima D327G mutant; [Troma][NTf₂]; In aq. acetate buffer; at 65 ℃; for 16h; pH=5; Solvent; Reagent/catalyst; regioselective reaction; Green chemistry; Enzymatic reaction;

DOI:10.1039/c5ra09301e

Reference yield:

2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl fluoride (439-03-2,439-04-3,439-05-4,2823-44-1,2823-46-3,3934-29-0,4163-45-5,20409-31-8,23235-96-3,51897-75-7,51897-76-8,51897-77-9,57573-38-3,62561-28-8,126641-47-2,4163-44-4) → C18H25NO13 (210832-21-6,335193-88-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium methylate / methanol

2: α-galactosidase from Bacteroides thetaiotaomicron D415G mutant; sodium formate / aq. buffer / 48 h / 30 °C / pH 6 / Enzymatic reaction

With α-galactosidase from Bacteroides thetaiotaomicron D415G mutant; sodium methylate; sodium formate; In methanol;

DOI:10.1111/febs.14018

upstream raw materials:

1-amido-1-deoxygalactopyranose

4-nitrophenyl-α-D-glucopyranoside

α-galactosyl fluoride

2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl fluoride