Methanesulfonic acid (4E,8Z)-10-benzyloxy-3,3,8-trimethyl-deca-4,8-dienyl ester

Base Information

Chemical Name:Methanesulfonic acid (4E,8Z)-10-benzyloxy-3,3,8-trimethyl-deca-4,8-dienyl ester
CAS No.:57074-08-5
Molecular Formula:C₂₁H₃₂O₄S
Molecular Weight:380.549
Hs Code.:

Synonyms:Methanesulfonic acid (4E,8Z)-10-benzyloxy-3,3,8-trimethyl-deca-4,8-dienyl ester

Suppliers and Price of Methanesulfonic acid (4E,8Z)-10-benzyloxy-3,3,8-trimethyl-deca-4,8-dienyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Methanesulfonic acid (4E,8Z)-10-benzyloxy-3,3,8-trimethyl-deca-4,8-dienyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Methanesulfonic acid (4E,8Z)-10-benzyloxy-3,3,8-trimethyl-deca-4,8-dienyl ester

There total 7 articles about Methanesulfonic acid (4E,8Z)-10-benzyloxy-3,3,8-trimethyl-deca-4,8-dienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 57074-07-4
(2Z,6E)-1-benzyloxy-3,8,8-trimethyldeca-2,6-dien-10-ol

: 124-63-0
methanesulfonyl chloride

: 57074-08-5
Methanesulfonic acid (4E,8Z)-10-benzyloxy-3,3,8-trimethyl-deca-4,8-dienyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1039/P19830001777

Reference yield:

: 55802-98-7
(2Z)-1-(benzyloxy)-3,7-dimethylocta-2,6-diene

: 57074-08-5
Methanesulfonic acid (4E,8Z)-10-benzyloxy-3,3,8-trimethyl-deca-4,8-dienyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 70 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 0 °C

2: 1.) sodium / 1.) EtOH, 2.) reflux, 3 h

3: m-chloroperbenzoic acid / CH₂Cl₂

4: 3.10 g / KOH / methanol / 1 h / Heating

5: 90 percent / 1.43M-n-BuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 20 min, 2.) room temperature, 2.5 h

6: 85 percent / 5.65percent Na(Hg) / tetrahydrofuran; methanol / 135.84 h / 20 °C

7: 100 percent / Et₃N / CH₂Cl₂ / 1 h / 0 °C

With potassium hydroxide; n-butyllithium; sodium amalgam; sodium; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1039/P19830001777

Reference yield:

: 87957-23-1,87957-24-2
2-<(Z)-1-phenylsulphonyl-6-benzyloxy-4-methylhex-4-enyl>-3,3-dimethyloxolane

: 57074-08-5
Methanesulfonic acid (4E,8Z)-10-benzyloxy-3,3,8-trimethyl-deca-4,8-dienyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 5.65percent Na(Hg) / tetrahydrofuran; methanol / 135.84 h / 20 °C

2: 100 percent / Et₃N / CH₂Cl₂ / 1 h / 0 °C

With sodium amalgam; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/P19830001777