3-O-[4-O-(4-iodobenzoyl-β-alanyl)-6-sulfo-α-D-quinovopyranosyl]-1,2-di-O-stearoyl-glycerol sodium salt

Base Information

Chemical Name:3-O-[4-O-(4-iodobenzoyl-β-alanyl)-6-sulfo-α-D-quinovopyranosyl]-1,2-di-O-stearoyl-glycerol sodium salt
CAS No.:1234307-16-4
Molecular Formula:C₅₅H₉₃INO₁₄S*Na
Molecular Weight:1174.3
Hs Code.:

Synonyms:3-O-[4-O-(4-iodobenzoyl-β-alanyl)-6-sulfo-α-D-quinovopyranosyl]-1,2-di-O-stearoyl-glycerol sodium salt

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Chemical Property of 3-O-[4-O-(4-iodobenzoyl-β-alanyl)-6-sulfo-α-D-quinovopyranosyl]-1,2-di-O-stearoyl-glycerol sodium salt

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Technology Process of 3-O-[4-O-(4-iodobenzoyl-β-alanyl)-6-sulfo-α-D-quinovopyranosyl]-1,2-di-O-stearoyl-glycerol sodium salt

There total 11 articles about 3-O-[4-O-(4-iodobenzoyl-β-alanyl)-6-sulfo-α-D-quinovopyranosyl]-1,2-di-O-stearoyl-glycerol sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.2%

: 1234307-15-3
3-O-[4-O-(β-alanyl)-6-sulfo-α-D-quinovopyranosyl]-1,2-di-O-stearoyl-glycerol sodium salt

: 97028-77-8
p-iodobenzoate de p-nitrophenol

: 1234307-16-4
3-O-[4-O-(4-iodobenzoyl-β-alanyl)-6-sulfo-α-D-quinovopyranosyl]-1,2-di-O-stearoyl-glycerol sodium salt

Guidance literature:: With pyridine; triethylamine; In dichloromethane; at 20 ℃; for 24h;

Reference yield:

: 2280-44-6
D-Glucose

: 1234307-16-4
3-O-[4-O-(4-iodobenzoyl-β-alanyl)-6-sulfo-α-D-quinovopyranosyl]-1,2-di-O-stearoyl-glycerol sodium salt

Guidance literature:: Multi-step reaction with 11 steps

1.1: trifluorormethanesulfonic acid / 48 h / 0 - 80 °C

1.2: 4 h / 40 °C

2.1: sodium hydroxide / N,N-dimethyl-formamide / 24 h / 20 °C

3.1: water; acetic acid / 1 h / Reflux

4.1: dmap; pyridine / 16 h / 0 °C

5.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; pyridine / dichloromethane / 18 h / 20 °C

6.1: N,N-dimethyl-formamide / 3 h / 90 °C

7.1: trimethylamine-N-oxide; water / osmium(VIII) oxide / tert-butyl alcohol / 24 h / 20 °C

8.1: pyridine / dichloromethane / 2 h / 20 °C

9.1: Oxone; potassium acetate; acetic acid / 48 h / 45 °C

10.1: hydrogen; acetic acid / palladium 10% on activated carbon / chloroform; methanol / 48 h / 20 °C

11.1: triethylamine; pyridine / dichloromethane / 24 h / 20 °C

With pyridine; dmap; Oxone; trimethylamine-N-oxide; trifluorormethanesulfonic acid; water; hydrogen; potassium acetate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; osmium(VIII) oxide; palladium 10% on activated carbon; In methanol; dichloromethane; chloroform; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 1234307-00-6
1-O-allyl-2,3-di-O-benzyl-4-O-(carbobenzoxy-β-alanyl)-6-O-tosyl-α-D-glucopyranoside

: 1234307-16-4
3-O-[4-O-(4-iodobenzoyl-β-alanyl)-6-sulfo-α-D-quinovopyranosyl]-1,2-di-O-stearoyl-glycerol sodium salt

Guidance literature:: Multi-step reaction with 6 steps

1: N,N-dimethyl-formamide / 3 h / 90 °C

2: trimethylamine-N-oxide; water / osmium(VIII) oxide / tert-butyl alcohol / 24 h / 20 °C

3: pyridine / dichloromethane / 2 h / 20 °C

4: Oxone; potassium acetate; acetic acid / 48 h / 45 °C

5: hydrogen; acetic acid / palladium 10% on activated carbon / chloroform; methanol / 48 h / 20 °C

6: triethylamine; pyridine / dichloromethane / 24 h / 20 °C

With pyridine; Oxone; trimethylamine-N-oxide; water; hydrogen; potassium acetate; acetic acid; triethylamine; osmium(VIII) oxide; palladium 10% on activated carbon; In methanol; dichloromethane; chloroform; N,N-dimethyl-formamide; tert-butyl alcohol;