[(3-Nitro-benzylaminooxalyl)-amino]-acetic acid 2-trimethylsilanyl-ethyl ester

Base Information

Chemical Name:[(3-Nitro-benzylaminooxalyl)-amino]-acetic acid 2-trimethylsilanyl-ethyl ester
CAS No.:187160-54-9
Molecular Formula:C₁₆H₂₃N₃O₆Si
Molecular Weight:381.461
Hs Code.:

Synonyms:[(3-Nitro-benzylaminooxalyl)-amino]-acetic acid 2-trimethylsilanyl-ethyl ester

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Chemical Property of [(3-Nitro-benzylaminooxalyl)-amino]-acetic acid 2-trimethylsilanyl-ethyl ester

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Technology Process of [(3-Nitro-benzylaminooxalyl)-amino]-acetic acid 2-trimethylsilanyl-ethyl ester

There total 5 articles about [(3-Nitro-benzylaminooxalyl)-amino]-acetic acid 2-trimethylsilanyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 112302-91-7
2-(trimethylsilyl)ethyl 2-aminoacetate

: 187160-53-8
N-(3-nitrobenzyl)-oxamic acid

: 187160-54-9
[(3-Nitro-benzylaminooxalyl)-amino]-acetic acid 2-trimethylsilanyl-ethyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 20h; Ambient temperature;
DOI:10.1021/jm960594+

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 187160-54-9
[(3-Nitro-benzylaminooxalyl)-amino]-acetic acid 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride, DMAP / CH₂Cl₂ / 19 h / Ambient temperature

2: H₂ / 10percent Pd/C / ethyl acetate / 4 h / Ambient temperature

3: 37 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride, DMAP / CH₂Cl₂ / 20 h / Ambient temperature

With dmap; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm960594+

Reference yield:

: 65057-56-9
2-(trimethylsilyl)ethyl 2-(((benzyloxy)carbonyl)amino)acetate

: 187160-54-9
[(3-Nitro-benzylaminooxalyl)-amino]-acetic acid 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethyl acetate / 4 h / Ambient temperature

2: 37 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride, DMAP / CH₂Cl₂ / 20 h / Ambient temperature

With dmap; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm960594+