1,3,2',6'-tetrakis(N-benzyloxycarbonyl)-3',4'-di-O-methoxymethylneamine

Base Information

Chemical Name:1,3,2',6'-tetrakis(N-benzyloxycarbonyl)-3',4'-di-O-methoxymethylneamine
CAS No.:419573-39-0
Molecular Formula:C₄₈H₅₈N₄O₁₆
Molecular Weight:947.006
Hs Code.:

Synonyms:1,3,2',6'-tetrakis(N-benzyloxycarbonyl)-3',4'-di-O-methoxymethylneamine

Suppliers and Price of 1,3,2',6'-tetrakis(N-benzyloxycarbonyl)-3',4'-di-O-methoxymethylneamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,3,2',6'-tetrakis(N-benzyloxycarbonyl)-3',4'-di-O-methoxymethylneamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,3,2',6'-tetrakis(N-benzyloxycarbonyl)-3',4'-di-O-methoxymethylneamine

There total 6 articles about 1,3,2',6'-tetrakis(N-benzyloxycarbonyl)-3',4'-di-O-methoxymethylneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 419573-38-9
1,3,2',6'-tetrakis(n-benzyloxycarbonyl)-5,6-O-cyclohexyl-3',4'-di-O-methoxymethylneamine

: 419573-39-0
1,3,2',6'-tetrakis(N-benzyloxycarbonyl)-3',4'-di-O-methoxymethylneamine

Guidance literature:: With acetic acid; In 1,4-dioxane; water; at 60 - 65 ℃; for 10h;
DOI:10.1021/ja011695m

Reference yield:

: 22854-75-7
N,N',N'',N'''-tetra(benzyloxycarbonyl)neamine

: 419573-39-0
1,3,2',6'-tetrakis(N-benzyloxycarbonyl)-3',4'-di-O-methoxymethylneamine

Guidance literature:: Multi-step reaction with 3 steps

1: 56.6 percent / TsOH / dimethylformamide / 36 h / 20 °C

2: 79 percent / Bu₄NI; (i-Pr)2NEt / dimethylformamide / 40 h / 32 °C

3: 95 percent / AcOH / dioxane; H₂O / 10 h / 60 - 65 °C

With tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja011695m

Reference yield:

: 3947-65-7
neomycin A

: 419573-39-0
1,3,2',6'-tetrakis(N-benzyloxycarbonyl)-3',4'-di-O-methoxymethylneamine

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / aq. Na₂CO₃ / acetone

2: 56.6 percent / TsOH / dimethylformamide / 36 h / 20 °C

3: 79 percent / Bu₄NI; (i-Pr)2NEt / dimethylformamide / 40 h / 32 °C

4: 95 percent / AcOH / dioxane; H₂O / 10 h / 60 - 65 °C

With tetra-(n-butyl)ammonium iodide; sodium carbonate; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ja011695m