methyl Z-3-(o-methoxyphenyl)-2-phenyl propenoate

Base Information

Chemical Name:methyl Z-3-(o-methoxyphenyl)-2-phenyl propenoate
CAS No.:261633-61-8
Molecular Formula:C₁₇H₁₆O₃
Molecular Weight:268.312
Hs Code.:

Synonyms:methyl Z-3-(o-methoxyphenyl)-2-phenyl propenoate

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Chemical Property of methyl Z-3-(o-methoxyphenyl)-2-phenyl propenoate

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Technology Process of methyl Z-3-(o-methoxyphenyl)-2-phenyl propenoate

There total 4 articles about methyl Z-3-(o-methoxyphenyl)-2-phenyl propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 955-10-2
3-phenylcumarin

: 74-88-4
methyl iodide

: 261633-61-8
methyl Z-3-(o-methoxyphenyl)-2-phenyl propenoate

Guidance literature:: 3-phenylcumarin; With potassium hydroxide; In dimethyl sulfoxide; at 40 ℃; for 0.025h;

methyl iodide; In dimethyl sulfoxide; at 20 ℃; for 1h;
DOI:10.1080/00397910008087187

Reference yield:

: 591-50-4
iodobenzene

: 84385-05-7
methyl (Z)-3-(2-methoxyphenyl)acrylate

: 261633-61-8
methyl Z-3-(o-methoxyphenyl)-2-phenyl propenoate

: (Z)-3-(2-methoxy-phenyl)-3-phenyl-acrylic acid methyl ester

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; silver(I) acetate; In N,N-dimethyl-formamide; at 80 ℃; for 72h; Inert atmosphere;
DOI:10.1055/s-0030-1259014

Reference yield:

: 955-10-2
3-phenylcumarin

: 261633-61-8
methyl Z-3-(o-methoxyphenyl)-2-phenyl propenoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: KOH / dimethylsulfoxide / 1.5 h / 40 °C

1.2: 69 percent / dimethylsulfoxide / 22 h / 20 °C

2.1: 100 percent

With potassium hydroxide; In dimethyl sulfoxide; 1.1: Ring cleavage / 1.2: Methylation / 2.1: Esterification;
DOI:10.1080/00397910008087187