C₂₇H₃₅O₄PZr

Base Information

• Chemical Name: C₂₇H₃₅O₄PZr
• CAS No.: 1569352-50-6
• Molecular Formula: C₂₇H₃₅O₄PZr
• Molecular Weight: 545.77
• Mol file: 1569352-50-6.mol

Synonyms:C₂₇H₃₅O₄PZr

Chemical Property of C₂₇H₃₅O₄PZr

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₂₇H₃₅O₄PZr

There total 1 articles about C₂₇H₃₅O₄PZr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-benzyloxy-but-1-ynyl)-phosphonic acid diethyl ester + zirconocene dichloride (1291-32-3) + ethylmagnesium bromide (925-90-6) → C27H35O4PZr (1569352-50-6)

Guidance literature:

zirconocene dichloride; ethylmagnesium bromide; In tetrahydrofuran; at -78 ℃; for 0.0833333h;

(4-benzyloxy-but-1-ynyl)-phosphonic acid diethyl ester; In tetrahydrofuran; at -78 - 20 ℃; for 2h; regioselective reaction;

DOI:10.1016/j.tetlet.2014.01.094

Reference yield:

oxalyl dichloride (79-37-8) + C27H35O4PZr (1569352-50-6) → C18H25O5P (1569352-41-5)

Guidance literature:

With copper(l) chloride; In tetrahydrofuran; at -30 - 0 ℃; for 1h; regioselective reaction;

DOI:10.1016/j.tetlet.2014.01.094

upstream raw materials:

zirconocene dichloride

ethylmagnesium bromide

Downstream raw materials:

C₁₈H₂₅O₅P