methyl 3,4-diacetoxybenzoate

Base Information

Chemical Name:methyl 3,4-diacetoxybenzoate
CAS No.:2239-98-7
Molecular Formula:C₁₂H₁₂O₆
Molecular Weight:252.224
Hs Code.:

Synonyms:methyl 3,4-diacetoxybenzoate

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Chemical Property of methyl 3,4-diacetoxybenzoate

Chemical Property:

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Technology Process of methyl 3,4-diacetoxybenzoate

There total 1 articles about methyl 3,4-diacetoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-50-3
3,4-Dihydroxybenzoic acid

: 2239-98-7
methyl 3,4-diacetoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 2 h / Reflux

2: pyridine / 0 - 20 °C

With pyridine; thionyl chloride;
DOI:10.1002/chem.201601361

Reference yield: 45.0%

: 2239-98-7
methyl 3,4-diacetoxybenzoate

: 168640-82-2
11-azido-3,6,9-trioxa-undecanyl p-toluenesulfonate

: methyl 4-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethoxy)-3-hydroxybenzoate

Guidance literature:: With potassium carbonate; In acetone; for 24h; Reflux;
DOI:10.1002/chem.201601361

Reference yield:

: 2239-98-7
methyl 3,4-diacetoxybenzoate

: 491-70-3
2-(3,4-Dihydroxy-phenyl)-5,7-dihydroxy-chromen-4-on

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / chloroform; N,N-dimethyl-formamide / Reflux

2.1: pyridine / 20 °C

3.1: potassium hydroxide / pyridine / 0.33 h / 50 °C

3.2: 0.5 h

3.3: Reflux

With thionyl chloride; potassium hydroxide; In pyridine; chloroform; N,N-dimethyl-formamide;
DOI:10.2174/1570178611999140206115633