(2S,4R)-5-biphenyl-4-yl-2-methyl-2-(tetrahydropyran-2-yloxymethyl)-4-[((1-trityl)-1H-[1,2,3]triazole-4-carbonyl)amino]pentanoic acid (5-methyl-2-oxo-[1,3]dioxol-4-yl)methyl ester

Base Information

Chemical Name:(2S,4R)-5-biphenyl-4-yl-2-methyl-2-(tetrahydropyran-2-yloxymethyl)-4-[((1-trityl)-1H-[1,2,3]triazole-4-carbonyl)amino]pentanoic acid (5-methyl-2-oxo-[1,3]dioxol-4-yl)methyl ester
CAS No.:1394050-32-8
Molecular Formula:C₅₁H₅₀N₄O₈
Molecular Weight:846.98
Hs Code.:

(2S,4R)-5-biphenyl-4-yl-2-methyl-2-(tetrahydropyran-2-yloxymethyl)-4-[((1-trityl)-1H-[1,2,3]triazole-4-carbonyl)amino]pentanoic acid (5-methyl-2-oxo-[1,3]dioxol-4-yl)methyl ester

Synonyms:(2S,4R)-5-biphenyl-4-yl-2-methyl-2-(tetrahydropyran-2-yloxymethyl)-4-[((1-trityl)-1H-[1,2,3]triazole-4-carbonyl)amino]pentanoic acid (5-methyl-2-oxo-[1,3]dioxol-4-yl)methyl ester

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Chemical Property of (2S,4R)-5-biphenyl-4-yl-2-methyl-2-(tetrahydropyran-2-yloxymethyl)-4-[((1-trityl)-1H-[1,2,3]triazole-4-carbonyl)amino]pentanoic acid (5-methyl-2-oxo-[1,3]dioxol-4-yl)methyl ester

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Technology Process of (2S,4R)-5-biphenyl-4-yl-2-methyl-2-(tetrahydropyran-2-yloxymethyl)-4-[((1-trityl)-1H-[1,2,3]triazole-4-carbonyl)amino]pentanoic acid (5-methyl-2-oxo-[1,3]dioxol-4-yl)methyl ester

There total 14 articles about (2S,4R)-5-biphenyl-4-yl-2-methyl-2-(tetrahydropyran-2-yloxymethyl)-4-[((1-trityl)-1H-[1,2,3]triazole-4-carbonyl)amino]pentanoic acid (5-methyl-2-oxo-[1,3]dioxol-4-yl)methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 146984-22-7
1-trityl-1H-1,2,3-triazole-4-carboxylic acid

: 1394050-44-2
C₂₉H₃₅NO₇

: 1394050-32-8
(2S,4R)-5-biphenyl-4-yl-2-methyl-2-(tetrahydropyran-2-yloxymethyl)-4-[((1-trityl)-1H-[1,2,3]triazole-4-carbonyl)amino]pentanoic acid (5-methyl-2-oxo-[1,3]dioxol-4-yl)methyl ester

Guidance literature:: 1-trityl-1H-1,2,3-triazole-4-carboxylic acid; With 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 ℃; for 0.25h; Inert atmosphere; Industry scale;

C₂₉H₃₅NO₇; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 1394050-32-8
(2S,4R)-5-biphenyl-4-yl-2-methyl-2-(tetrahydropyran-2-yloxymethyl)-4-[((1-trityl)-1H-[1,2,3]triazole-4-carbonyl)amino]pentanoic acid (5-methyl-2-oxo-[1,3]dioxol-4-yl)methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / dichloromethane / 18 h / 0 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V) / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere; Industry scale

2.2: 0.5 h / 0 °C / Inert atmosphere

With 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); N-ethyl-N,N-diisopropylamine; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1394050-43-1
(2S,4R)-4-amino-5-biphenyl-4-yl-2-(hydroxymethyl)-2-methylpentanoic acid (5-methyl-2-oxo-[1,3]dioxol-4-yl)methyl ester

: 1394050-32-8
(2S,4R)-5-biphenyl-4-yl-2-methyl-2-(tetrahydropyran-2-yloxymethyl)-4-[((1-trityl)-1H-[1,2,3]triazole-4-carbonyl)amino]pentanoic acid (5-methyl-2-oxo-[1,3]dioxol-4-yl)methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / dichloromethane / 18 h / 0 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V) / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere; Industry scale

2.2: 0.5 h / 0 °C / Inert atmosphere

With 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); N-ethyl-N,N-diisopropylamine; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;