4-<4-(dimethylamino)benzoyl>-1-methyl-1H-pyrrole-2-carboxaldehyde

Base Information

Chemical Name:4-<4-(dimethylamino)benzoyl>-1-methyl-1H-pyrrole-2-carboxaldehyde
CAS No.:128843-63-0
Molecular Formula:C₁₅H₁₆N₂O₂
Molecular Weight:256.304
Hs Code.:

Synonyms:4-<4-(dimethylamino)benzoyl>-1-methyl-1H-pyrrole-2-carboxaldehyde

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Chemical Property of 4-<4-(dimethylamino)benzoyl>-1-methyl-1H-pyrrole-2-carboxaldehyde

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Technology Process of 4-<4-(dimethylamino)benzoyl>-1-methyl-1H-pyrrole-2-carboxaldehyde

There total 4 articles about 4-<4-(dimethylamino)benzoyl>-1-methyl-1H-pyrrole-2-carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 128843-59-4
1-Methyl-4-(4-nitro-benzoyl)-1H-pyrrole-2-carbaldehyde

: 128843-63-0
4-<4-(dimethylamino)benzoyl>-1-methyl-1H-pyrrole-2-carboxaldehyde

Guidance literature:: With hydrogen; palladium on activated charcoal; In water; acetic acid; at 50 ℃; for 5h; under 2585.7 Torr;
DOI:10.1021/jm00172a026

Reference yield:

: 96-54-8
N-Methylpyrrole

: 4755-50-4
4-(dimethylamino)benzoyl chloride

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 128843-63-0
4-<4-(dimethylamino)benzoyl>-1-methyl-1H-pyrrole-2-carboxaldehyde

Guidance literature:: N-Methylpyrrole; N,N-dimethyl-formamide; With oxalyl dichloride; In 1,2-dichloro-ethane; at 0 ℃;

4-(dimethylamino)benzoyl chloride; With aluminium trichloride; In 1,2-dichloro-ethane; at 20 ℃;

In 1,2-dichloro-ethane; at 20 ℃; Further stages.;
DOI:10.1021/jm015515v

Reference yield:

: 96-54-8
N-Methylpyrrole

: 128843-63-0
4-<4-(dimethylamino)benzoyl>-1-methyl-1H-pyrrole-2-carboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / 1,2-dichloro-ethane / 0.25 h / 20 °C

2: AlCl₃ / 1,2-dichloro-ethane / 3 h

With aluminium trichloride; oxalyl dichloride; In 1,2-dichloro-ethane; 1: Vilsmeier-Haack reaction / 2: Friedel-Crafts reaction;
DOI:10.1021/jm021070e