Os(C₁₀H₈N₂)2(C₇H₄NOC₆H₄O)⁽¹⁺⁾*PF₆^(1-)=Os(C₁₀H₈N₂)2(C₇H₄NOC₆H₄O)PF₆

Base Information

• Chemical Name: Os(C₁₀H₈N₂)2(C₇H₄NOC₆H₄O)⁽¹⁺⁾*PF₆^(1-)=Os(C₁₀H₈N₂)2(C₇H₄NOC₆H₄O)PF₆
• CAS No.: 477217-33-7
• Molecular Formula: C₃₃H₂₄N₅O₂Os*F₆P
• Molecular Weight: 857.75
• Mol file: 477217-33-7.mol

Synonyms:Os(C₁₀H₈N₂)2(C₇H₄NOC₆H₄O)⁽¹⁺⁾*PF₆^(1-)=Os(C₁₀H₈N₂)2(C₇H₄NOC₆H₄O)PF₆

Chemical Property of Os(C₁₀H₈N₂)2(C₇H₄NOC₆H₄O)⁽¹⁺⁾*PF₆^(1-)=Os(C₁₀H₈N₂)2(C₇H₄NOC₆H₄O)PF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of Os(C₁₀H₈N₂)2(C₇H₄NOC₆H₄O)⁽¹⁺⁾*PF₆^(1-)=Os(C₁₀H₈N₂)2(C₇H₄NOC₆H₄O)PF₆

There total 1 articles about Os(C₁₀H₈N₂)2(C₇H₄NOC₆H₄O)⁽¹⁺⁾*PF₆^(1-)=Os(C₁₀H₈N₂)2(C₇H₄NOC₆H₄O)PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

ammonium hexafluorophosphate + bis(2,2'-bipyridine)osmium(II) dichloride (15702-72-4,79982-56-2) + 2-(2-Hydroxyphenyl)benzoxazole (835-64-3) → Os(C10H8N2)2(C7H4NOC6H4O)(1+)*PF6(1-)=Os(C10H8N2)2(C7H4NOC6H4O)PF6 (477217-33-7)

Guidance literature:

With diethylamine; In ethanol; water; a soln. of benzoxazole in ethanol/water (2% diethylamine) was slowly added to a heated soln. of complex in the same solvent over 20 min, the mixt. was heated under reflux under Ar for 8 h; neutralized with H2SO4, the soln. was allowed to stand for several h, filtered, few drops of aq. NH4PF6 were added, crystals were filtered; elem. anal.;

DOI:10.1021/ic0202561

upstream raw materials:

bis(2,2'-bipyridine)osmium(II) dichloride

2-(2-Hydroxyphenyl)benzoxazole