2,3-di-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside-N-phenyl-trifluoroacetimidate

Base Information

Chemical Name:2,3-di-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside-N-phenyl-trifluoroacetimidate
CAS No.:1334540-26-9
Molecular Formula:C₃₅H₃₀F₃NO₇
Molecular Weight:633.621
Hs Code.:

Synonyms:2,3-di-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside-N-phenyl-trifluoroacetimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-di-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside-N-phenyl-trifluoroacetimidate

Chemical Property:

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Technology Process of 2,3-di-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside-N-phenyl-trifluoroacetimidate

There total 2 articles about 2,3-di-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside-N-phenyl-trifluoroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421758-33-9
C₂₇H₂₆O₇

: 61881-19-4
2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

: 1334540-26-9
2,3-di-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside-N-phenyl-trifluoroacetimidate

Guidance literature:: With caesium carbonate; In dichloromethane; at 0 - 20 ℃;
DOI:10.1039/c1cc13614c

Reference yield:

: 98-88-4
benzoyl chloride

: 1334540-26-9
2,3-di-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside-N-phenyl-trifluoroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; dmap / dichloromethane / 0 - 20 °C

2: ammonium cerium (IV) nitrate; water / acetonitrile / 2 h

3: caesium carbonate / dichloromethane / 0 - 20 °C

With pyridine; dmap; ammonium cerium (IV) nitrate; water; caesium carbonate; In dichloromethane; acetonitrile;
DOI:10.1039/c1cc13614c

Reference yield: 94.0%

: 920958-49-2
benzyl-(5-hydroxy-pentyl)-carbamic acid benzyl ester

: 1334540-26-9
2,3-di-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside-N-phenyl-trifluoroacetimidate

: 1421768-15-1
N-(benzyl)benzyloxycarbonyl-5-aminopentanyl 2,3-di-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 - -20 ℃; for 1h; Inert atmosphere; Molecular sieve;