Technology Process of C26H48O2Si2
There total 7 articles about C26H48O2Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at -78 - 0 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1039/c3cc45170d
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: cerium(III) chloride heptahydrate; sodium tetrahydroborate / methanol / -78 - -30 °C / Inert atmosphere
2.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
3.1: diisobutylaluminium hydride / toluene / 0.67 h / -78 °C / Inert atmosphere
3.2: sat. Na/K tartrate / 2 h / 20 °C / Inert atmosphere
4.1: tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
6.1: triethylamine; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / -78 - 0 °C / Inert atmosphere
With
sodium tetrahydroborate; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1039/c3cc45170d
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
2.1: diisobutylaluminium hydride / toluene / 0.67 h / -78 °C / Inert atmosphere
2.2: sat. Na/K tartrate / 2 h / 20 °C / Inert atmosphere
3.1: tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
5.1: triethylamine; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / -78 - 0 °C / Inert atmosphere
With
tetrabutyl ammonium fluoride; diisobutylaluminium hydride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1039/c3cc45170d