ethyl 3-(p-tolyl)-1H-pyrrole-2-carboxylate

Base Information

Chemical Name:ethyl 3-(p-tolyl)-1H-pyrrole-2-carboxylate
CAS No.:1443446-77-2
Molecular Formula:C₁₄H₁₅NO₂
Molecular Weight:229.279
Hs Code.:

Synonyms:ethyl 3-(p-tolyl)-1H-pyrrole-2-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 3-(p-tolyl)-1H-pyrrole-2-carboxylate

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Technology Process of ethyl 3-(p-tolyl)-1H-pyrrole-2-carboxylate

There total 1 articles about ethyl 3-(p-tolyl)-1H-pyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 2999-46-4
Ethyl isocyanoacetate

: 766-97-2
4-n-methylphenylacetylene

: 1443446-77-2
ethyl 3-(p-tolyl)-1H-pyrrole-2-carboxylate

Guidance literature:: With silver carbonate; In 1-methyl-pyrrolidin-2-one; at 80 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201302604

Reference yield:

: 1443446-77-2
ethyl 3-(p-tolyl)-1H-pyrrole-2-carboxylate

: 1604040-72-3
C₁₂H₁₃N

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; Reflux; Inert atmosphere;
DOI:10.1021/ja5028138

Reference yield:

: 1443446-77-2
ethyl 3-(p-tolyl)-1H-pyrrole-2-carboxylate

: 1604040-76-7
C₁₃H₁₃NO

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux; Inert atmosphere

2: trichlorophosphate / 0 - 40 °C / Inert atmosphere

With lithium aluminium tetrahydride; trichlorophosphate; In tetrahydrofuran;
DOI:10.1021/ja5028138