[N⁽³⁾,N⁽³⁾-dimethyl-N⁽¹⁾-(1-naphthyl)-N⁽¹⁾-phenyl]-3-aminothioacrylamide

Base Information

• Chemical Name: [N⁽³⁾,N⁽³⁾-dimethyl-N⁽¹⁾-(1-naphthyl)-N⁽¹⁾-phenyl]-3-aminothioacrylamide
• CAS No.: 864053-47-4
• Molecular Formula: C₂₁H₂₀N₂S
• Molecular Weight: 332.469

Synonyms:[N⁽³⁾,N⁽³⁾-dimethyl-N⁽¹⁾-(1-naphthyl)-N⁽¹⁾-phenyl]-3-aminothioacrylamide

Chemical Property of [N⁽³⁾,N⁽³⁾-dimethyl-N⁽¹⁾-(1-naphthyl)-N⁽¹⁾-phenyl]-3-aminothioacrylamide

Chemical Property:

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Technology Process of [N⁽³⁾,N⁽³⁾-dimethyl-N⁽¹⁾-(1-naphthyl)-N⁽¹⁾-phenyl]-3-aminothioacrylamide

There total 1 articles about [N⁽³⁾,N⁽³⁾-dimethyl-N⁽¹⁾-(1-naphthyl)-N⁽¹⁾-phenyl]-3-aminothioacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

1-chloro-3-dimethylamino-1-(N-(1-naphthyl)-N-phenyl)propeniminium perchlorate → [N(3),N(3)-dimethyl-N(1)-(1-naphthyl)-N(1)-phenyl]-3-aminothioacrylamide (864053-47-4)

Guidance literature:

With sodium sulfide; In water; acetonitrile; at 20 ℃;

DOI:10.1021/jo0503097

Reference yield: 38.0%

1,3-Dichloroacetone (534-07-6) + [N(3),N(3)-dimethyl-N(1)-(1-naphthyl)-N(1)-phenyl]-3-aminothioacrylamide (864053-47-4) → bis-[5-(naphthalen-1-yl-phenyl-amino)-thiophen-2-yl]-methanone

Guidance literature:

1,3-Dichloroacetone; [N⁽³⁾,N⁽³⁾-dimethyl-N⁽¹⁾-(1-naphthyl)-N⁽¹⁾-phenyl]-3-aminothioacrylamide; In acetonitrile; for 0.0333333h; Heating;

With triethylamine; In acetonitrile;

DOI:10.1016/S0040-4020(02)00083-2

Reference yield:

[N(3),N(3)-dimethyl-N(1)-(1-naphthyl)-N(1)-phenyl]-3-aminothioacrylamide (864053-47-4) → 1-[5-(naphthalen-1-yl-phenyl-amino)-thiophen-2-yl]-ethanone

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / 3 h / Heating

2: Et₃N / acetonitrile

With triethylamine; In acetonitrile;

DOI:10.1016/S0040-4020(02)00083-2

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