mesityl 2-pyridyl ketone

Base Information

Chemical Name:mesityl 2-pyridyl ketone
CAS No.:126939-66-0
Molecular Formula:C₁₅H₁₅NO
Molecular Weight:225.29
Hs Code.:

Synonyms:mesityl 2-pyridyl ketone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of mesityl 2-pyridyl ketone

Chemical Property:

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Technology Process of mesityl 2-pyridyl ketone

There total 6 articles about mesityl 2-pyridyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 17971-25-4
mesityl(pyridine-2-yl)methanol

: 126939-66-0
mesityl 2-pyridyl ketone

Guidance literature:: With dicarbonyl(cyclopentadienyl)iron(II) chloride; sodium hydride; In toluene; for 20h; Reflux; Inert atmosphere; Schlenk technique;
DOI:10.1039/c4cc01498g

Reference yield:

: 65231-46-1
C-pyridin-2-yl-C-(2,4,6-trimethyl-phenyl)-methyleneamine

: 126939-66-0
mesityl 2-pyridyl ketone

Guidance literature:: With hydrogenchloride; at 90 ℃;

Reference yield:

: 576-83-0
2,4,6-trimethylphenyl bromide

: 2-picolylcarbonate

: 126939-66-0
mesityl 2-pyridyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium / tetrahydrofuran; diethyl ether / 0.5 h / 0 - 50 °C / Inert atmosphere; Schlenk technique

1.2: 0 °C / Inert atmosphere; Schlenk technique

2.1: dicarbonyl(cyclopentadienyl)iron(II) chloride; sodium hydride / toluene / 20 h / Reflux; Inert atmosphere; Schlenk technique

With dicarbonyl(cyclopentadienyl)iron(II) chloride; sodium hydride; magnesium; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1039/c4cc01498g