Hexyl-[1-pyridin-2-yl-1-(2,4,6-trimethyl-phenyl)-meth-(Z)-ylidene]-amine

Base Information

Chemical Name:Hexyl-[1-pyridin-2-yl-1-(2,4,6-trimethyl-phenyl)-meth-(Z)-ylidene]-amine
CAS No.:126939-67-1
Molecular Formula:C₂₁H₂₈N₂
Molecular Weight:308.467
Hs Code.:

Synonyms:Hexyl-[1-pyridin-2-yl-1-(2,4,6-trimethyl-phenyl)-meth-(Z)-ylidene]-amine

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Chemical Property of Hexyl-[1-pyridin-2-yl-1-(2,4,6-trimethyl-phenyl)-meth-(Z)-ylidene]-amine

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Technology Process of Hexyl-[1-pyridin-2-yl-1-(2,4,6-trimethyl-phenyl)-meth-(Z)-ylidene]-amine

There total 2 articles about Hexyl-[1-pyridin-2-yl-1-(2,4,6-trimethyl-phenyl)-meth-(Z)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 111-26-2
hexan-1-amine

: 126939-66-0
mesityl 2-pyridyl ketone

: 126939-67-1
Hexyl-[1-pyridin-2-yl-1-(2,4,6-trimethyl-phenyl)-meth-(Z)-ylidene]-amine

Guidance literature:: titanium tetrachloride; In toluene; for 12h; Heating;
DOI:10.1016/S0040-4039(01)93488-4

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 126939-67-1
Hexyl-[1-pyridin-2-yl-1-(2,4,6-trimethyl-phenyl)-meth-(Z)-ylidene]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) CrO₃-pyridine

2: 80 percent / TiCl₄ / toluene / 12 h / Heating

With chromium trioxide-pyridine complex; titanium tetrachloride; In toluene;
DOI:10.1016/S0040-4039(01)93488-4

Reference yield:

: 126939-67-1
Hexyl-[1-pyridin-2-yl-1-(2,4,6-trimethyl-phenyl)-meth-(Z)-ylidene]-amine

: 74-88-4
methyl iodide

: 123-82-0
2-heptylamine

Guidance literature:: With hydrogenchloride; lithium diisopropyl amide; Multistep reaction; 1.) 5 min, THF, 2.) 12 h, RT, 3.) 2-3 d, reflux;
DOI:10.1016/S0040-4039(01)93488-4