2-N-benzyl-5-N-[4⁽²⁴⁾,6⁽¹⁰⁾,12⁽¹⁶⁾,18⁽²²⁾-tetramethylenedioxy-2,8,14,20-tetrapentylresorcin[4]arene-5-yl]imidazolinium bromide

Base Information

• Chemical Name: 2-N-benzyl-5-N-[4⁽²⁴⁾,6⁽¹⁰⁾,12⁽¹⁶⁾,18⁽²²⁾-tetramethylenedioxy-2,8,14,20-tetrapentylresorcin[4]arene-5-yl]imidazolinium bromide
• CAS No.: 1449509-01-6
• Molecular Formula: Br*C₆₂H₇₃N₂O₈
• Molecular Weight: 1054.17

Synonyms:2-N-benzyl-5-N-[4⁽²⁴⁾,6⁽¹⁰⁾,12⁽¹⁶⁾,18⁽²²⁾-tetramethylenedioxy-2,8,14,20-tetrapentylresorcin[4]arene-5-yl]imidazolinium bromide

Chemical Property of 2-N-benzyl-5-N-[4⁽²⁴⁾,6⁽¹⁰⁾,12⁽¹⁶⁾,18⁽²²⁾-tetramethylenedioxy-2,8,14,20-tetrapentylresorcin[4]arene-5-yl]imidazolinium bromide

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Technology Process of 2-N-benzyl-5-N-[4⁽²⁴⁾,6⁽¹⁰⁾,12⁽¹⁶⁾,18⁽²²⁾-tetramethylenedioxy-2,8,14,20-tetrapentylresorcin[4]arene-5-yl]imidazolinium bromide

There total 1 articles about 2-N-benzyl-5-N-[4⁽²⁴⁾,6⁽¹⁰⁾,12⁽¹⁶⁾,18⁽²²⁾-tetramethylenedioxy-2,8,14,20-tetrapentylresorcin[4]arene-5-yl]imidazolinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

5-(imidazol-1-yl)-4(24),6(10),12(16),18(22)-tetramethylenedioxy-2,8,14,20-tetrapentylresorcin[4]arene + benzyl bromide (100-39-0) → 2-N-benzyl-5-N-[4(24),6(10),12(16),18(22)-tetramethylenedioxy-2,8,14,20-tetrapentylresorcin[4]arene-5-yl]imidazolinium bromide (1449509-01-6)

Guidance literature:

In chloroform; for 48h; Inert atmosphere; Reflux;

DOI:10.1002/cctc.201200716

Reference yield: 79.0%

bis[(benzyldimethylamino)chloropalladium(II)] + 2-N-benzyl-5-N-[4(24),6(10),12(16),18(22)-tetramethylenedioxy-2,8,14,20-tetrapentylresorcin[4]arene-5-yl]imidazolinium bromide (1449509-01-6) → C71H84ClN3O8Pd

Guidance literature:

With potassium carbonate; In acetonitrile; at 80 ℃; for 16h; Inert atmosphere;

DOI:10.1002/cctc.201200716

Reference yield: 75.0%

pyridine (110-86-1) + 2-N-benzyl-5-N-[4(24),6(10),12(16),18(22)-tetramethylenedioxy-2,8,14,20-tetrapentylresorcin[4]arene-5-yl]imidazolinium bromide (1449509-01-6) + potassium bromide (7558-02-3,7758-02-3) + palladium dichloride → trans-dibromo-[2-{4(24),6(10),12(16),18(22)-tetramethylenedioxy-2,8,14,20-tetrapentylresorcin[4]aren-5-yl}-5-benzylimidazol-2-yliden]pyridine palladium(II)

Guidance literature:

With potassium carbonate; at 80 ℃; for 17h; Inert atmosphere;

DOI:10.1002/cctc.201200716

upstream raw materials:

benzyl bromide

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