2,3-bis(trifluoromethyl)-1,4-diphenyl-7,7-dimethyl-7-silanorbornadiene

Base Information

• Chemical Name: 2,3-bis(trifluoromethyl)-1,4-diphenyl-7,7-dimethyl-7-silanorbornadiene
• CAS No.: 38361-48-7
• Molecular Formula: C₂₂H₁₈F₆Si
• Molecular Weight: 424.461
• Mol file: 38361-48-7.mol

Synonyms:2,3-bis(trifluoromethyl)-1,4-diphenyl-7,7-dimethyl-7-silanorbornadiene

Chemical Property of 2,3-bis(trifluoromethyl)-1,4-diphenyl-7,7-dimethyl-7-silanorbornadiene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-bis(trifluoromethyl)-1,4-diphenyl-7,7-dimethyl-7-silanorbornadiene

There total 2 articles about 2,3-bis(trifluoromethyl)-1,4-diphenyl-7,7-dimethyl-7-silanorbornadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

hexafluoro-2-butyne (692-50-2) + 1,1-dimethyl-2,5-diphenylsilole (7688-03-1) → 2,3-bis(trifluoromethyl)-1,4-diphenyl-7,7-dimethyl-7-silanorbornadiene (38361-48-7)

Guidance literature:

In chloroform; for 120h; Ambient temperature;

DOI:10.1016/S0022-328X(00)86813-8

Reference yield:

→ 2,3-bis(trifluoromethyl)-1,4-diphenyl-7,7-dimethyl-7-silanorbornadiene (38361-48-7)

Guidance literature:

1,1-Dimethyl-2,5-diphenyl-1-silacyclopentadien, Perfluor-2-butin;

DOI:10.1021/ja00772a069

Reference yield: 69.0%

2,3-bis(trifluoromethyl)-1,4-diphenyl-7,7-dimethyl-7-silanorbornadiene (38361-48-7) → dimethyldifluorosilane (353-66-2) + 7,7,8,8-Tetrafluoro-2,5-diphenyl-bicyclo[4.2.0]octa-1,3,5-triene (38361-49-8)

Guidance literature:

at 180 ℃; photolytic and/or pyrolytic behaviour; other 7-silanorbornadienes, var. conditions;

DOI:10.1016/S0022-328X(00)86813-8

upstream raw materials:

hexafluoro-2-butyne

1,1-dimethyl-2,5-diphenylsilole

Downstream raw materials:

(1,4-Diphenyl-5,6-bis-trifluoromethyl-cyclohexa-2,4-dienyl)-dimethyl-silanol

dimethyldifluorosilane

7,7,8,8-Tetrafluoro-2,5-diphenyl-bicyclo[4.2.0]octa-1,3,5-triene

9,9-Difluoro-2-phenyl-1-trifluoromethyl-9H-fluorene