Technology Process of 2-methoxydibenzo[b,d]thiophene 5,5-dioxide
There total 4 articles about 2-methoxydibenzo[b,d]thiophene 5,5-dioxide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetone;
for 2h;
Schlenk technique;
Inert atmosphere;
Reflux;
DOI:10.1021/acs.orglett.5b03384
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetic acid; dihydrogen peroxide / 12 h / Reflux
2: potassium hydroxide; tris-(dibenzylideneacetone)dipalladium(0); tert-butyl XPhos / water; 1,4-dioxane / 16 h / 100 °C / Schlenk technique; Inert atmosphere
3: potassium carbonate / acetone / 2 h / Schlenk technique; Inert atmosphere; Reflux
With
tris-(dibenzylideneacetone)dipalladium(0); dihydrogen peroxide; potassium carbonate; acetic acid; potassium hydroxide; tert-butyl XPhos;
In
1,4-dioxane; water; acetone;
DOI:10.1021/acs.orglett.5b03384
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium hydroxide; tris-(dibenzylideneacetone)dipalladium(0); tert-butyl XPhos / water; 1,4-dioxane / 16 h / 100 °C / Schlenk technique; Inert atmosphere
2: potassium carbonate / acetone / 2 h / Schlenk technique; Inert atmosphere; Reflux
With
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate; potassium hydroxide; tert-butyl XPhos;
In
1,4-dioxane; water; acetone;
DOI:10.1021/acs.orglett.5b03384
