4-(((2,2,2-trichloroethoxy)carbonyloxy)methyl)benzyl N-benzyl-N-(5-((2,3-dimethylbutan-2-yl)dimethylsilyloxy)pentyl)carbamate

Base Information

Chemical Name:4-(((2,2,2-trichloroethoxy)carbonyloxy)methyl)benzyl N-benzyl-N-(5-((2,3-dimethylbutan-2-yl)dimethylsilyloxy)pentyl)carbamate
CAS No.:1276114-10-3
Molecular Formula:C₃₂H₄₆Cl₃NO₆Si
Molecular Weight:675.165
Hs Code.:

Synonyms:4-(((2,2,2-trichloroethoxy)carbonyloxy)methyl)benzyl N-benzyl-N-(5-((2,3-dimethylbutan-2-yl)dimethylsilyloxy)pentyl)carbamate

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Chemical Property of 4-(((2,2,2-trichloroethoxy)carbonyloxy)methyl)benzyl N-benzyl-N-(5-((2,3-dimethylbutan-2-yl)dimethylsilyloxy)pentyl)carbamate

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Technology Process of 4-(((2,2,2-trichloroethoxy)carbonyloxy)methyl)benzyl N-benzyl-N-(5-((2,3-dimethylbutan-2-yl)dimethylsilyloxy)pentyl)carbamate

There total 5 articles about 4-(((2,2,2-trichloroethoxy)carbonyloxy)methyl)benzyl N-benzyl-N-(5-((2,3-dimethylbutan-2-yl)dimethylsilyloxy)pentyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1276114-07-8
N-benzyl-5-((2,3-dimethylbutan-2-yl)dimethylsilyloxy)pentan-1-amine

: C₁₈H₁₄Cl₃NO₇

: 1276114-10-3
4-(((2,2,2-trichloroethoxy)carbonyloxy)methyl)benzyl N-benzyl-N-(5-((2,3-dimethylbutan-2-yl)dimethylsilyloxy)pentyl)carbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃;
DOI:10.1039/c0cc04686h

Reference yield:

: 1276114-08-9
4-(hydroxymethyl)benzyl 2,2,2-trichloroethylcarbonate

: 1276114-10-3
4-(((2,2,2-trichloroethoxy)carbonyloxy)methyl)benzyl N-benzyl-N-(5-((2,3-dimethylbutan-2-yl)dimethylsilyloxy)pentyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 °C

With pyridine; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c0cc04686h

Reference yield:

: 67373-56-2
chlorodimethyl(1,1,2-trimethylpropyl)silane

: 1276114-10-3
4-(((2,2,2-trichloroethoxy)carbonyloxy)methyl)benzyl N-benzyl-N-(5-((2,3-dimethylbutan-2-yl)dimethylsilyloxy)pentyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 0 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 °C

With 1H-imidazole; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1039/c0cc04686h