C₁₉H₂₂ClNO₅*ClH

Base Information

Chemical Name:C₁₉H₂₂ClNO₅*ClH
CAS No.:1416443-75-8
Molecular Formula:C₁₉H₂₂ClNO₅*ClH
Molecular Weight:416.301
Hs Code.:

C<sub>19</sub>H<sub>22</sub>ClNO<sub>5</sub>*ClH

Synonyms:C₁₉H₂₂ClNO₅*ClH

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Chemical Property of C₁₉H₂₂ClNO₅*ClH

Chemical Property:

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Technology Process of C₁₉H₂₂ClNO₅*ClH

There total 14 articles about C₁₉H₂₂ClNO₅*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1416443-90-7
(S)-2-[((2-(2,6-dimethoxyphenoxy)ethyl)amino)methyl]-8-chloro-1,4-benzodioxane

: 1416443-75-8
C₁₉H₂₂ClNO₅*ClH

Guidance literature:: With hydrogenchloride; In ethanol; water;
DOI:10.1016/j.ejmech.2012.09.049

Reference yield:

: 4525-75-1
2-chlorophenyl acetate

: 1416443-75-8
C₁₉H₂₂ClNO₅*ClH

Guidance literature:: Multi-step reaction with 11 steps

1: aluminum (III) chloride / 1,2-dichloro-benzene / 5 h / 20 - 100 °C

2: tetrabutylammomium bromide; sodium hydroxide / water / 5 h / 20 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 168 h / 0 - 20 °C

4: water; sodium hydroxide / methanol / 2 h

5: potassium carbonate / N,N-dimethyl-formamide / 4 h

6: hydrogenchloride / ethanol; water / 4 h / 75 °C

7: triethylamine / dichloromethane / 2 h / 0 - 5 °C

8: palladium on activated charcoal; hydrogen / methanol / 20 °C

9: potassium carbonate / acetone / 24 h / Reflux

10: 2-methyl-propan-1-ol / 24 h / Reflux

11: hydrogenchloride / ethanol; water

With hydrogenchloride; aluminum (III) chloride; palladium on activated charcoal; tetrabutylammomium bromide; water; hydrogen; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In methanol; ethanol; dichloromethane; 2-methyl-propan-1-ol; water; N,N-dimethyl-formamide; 1,2-dichloro-benzene; acetone; 1: |Fries Phenol Ester Rearrangement / 3: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1016/j.ejmech.2012.09.049

Reference yield:

: 95-57-8
2-monochlorophenol

: 1416443-75-8
C₁₉H₂₂ClNO₅*ClH

Guidance literature:: Multi-step reaction with 12 steps

1: pyridine / dichloromethane / 4 h / 20 - 25 °C

2: aluminum (III) chloride / 1,2-dichloro-benzene / 5 h / 20 - 100 °C

3: tetrabutylammomium bromide; sodium hydroxide / water / 5 h / 20 °C

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 168 h / 0 - 20 °C

5: water; sodium hydroxide / methanol / 2 h

6: potassium carbonate / N,N-dimethyl-formamide / 4 h

7: hydrogenchloride / ethanol; water / 4 h / 75 °C

8: triethylamine / dichloromethane / 2 h / 0 - 5 °C

9: palladium on activated charcoal; hydrogen / methanol / 20 °C

10: potassium carbonate / acetone / 24 h / Reflux

11: 2-methyl-propan-1-ol / 24 h / Reflux

12: hydrogenchloride / ethanol; water

With pyridine; hydrogenchloride; aluminum (III) chloride; palladium on activated charcoal; tetrabutylammomium bromide; water; hydrogen; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In methanol; ethanol; dichloromethane; 2-methyl-propan-1-ol; water; N,N-dimethyl-formamide; 1,2-dichloro-benzene; acetone; 2: |Fries Phenol Ester Rearrangement / 4: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1016/j.ejmech.2012.09.049