Technology Process of C20H29ClINO5
There total 7 articles about C20H29ClINO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran;
at 20 ℃;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: silver trifluoroacetate; iodine / chloroform / 120 h / -60 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C
3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 20 °C / Cooling with ice
With
tetrabutyl ammonium fluoride; iodine; silver trifluoroacetate; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; chloroform;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N,N-dimethylformamide dineopentyl acetal / toluene / 3 h / Reflux
2: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C
3: silver trifluoroacetate; iodine / chloroform / 120 h / -60 °C
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C
5: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 20 °C / Cooling with ice
With
1H-imidazole; tetrabutyl ammonium fluoride; iodine; silver trifluoroacetate; triphenylphosphine; N,N-dimethylformamide dineopentyl acetal; diethylazodicarboxylate;
In
tetrahydrofuran; chloroform; N,N-dimethyl-formamide; toluene;