(1R)-menthyl trichloroacetate

Base Information

Chemical Name:(1R)-menthyl trichloroacetate
CAS No.:157319-27-2
Molecular Formula:C₁₂H₁₉Cl₃O₂
Molecular Weight:301.641
Hs Code.:

Synonyms:(1R)-menthyl trichloroacetate

Suppliers and Price of (1R)-menthyl trichloroacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1R)-menthyl trichloroacetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1R)-menthyl trichloroacetate

There total 1 articles about (1R)-menthyl trichloroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 2216-51-5
(-)-menthol

: 76-02-8
trifluoroacetyl chloride

: 157319-27-2
(1R)-menthyl trichloroacetate

Guidance literature:: With pyridine; In diethyl ether; at 0 - 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tetlet.2013.10.044

Reference yield: 26.0%

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 157319-27-2
(1R)-menthyl trichloroacetate

: nonacarbonyl-μ3-(menthyloxycarbonyl-methylidine)-triangulo-tricobalt (3 Co-Co)

Guidance literature:: In acetone; Co2(CO)8 stirred in acetone for 1 h at room temp., menthylester added, heated slowly to 60°C, stirred for 4 h at 60°C; solv. removed in vac., extd. 4 times with hexane, washed with water, dried with MgSO4 overnight, filtered, concd. in vac., chromy., concd., crystd. at room temp.; elem.anal.;