Acetic acid 2-acetoxy-3-[3-(2-acetoxy-1-acetoxymethyl-ethylcarbamoyl)-5-diacetylamino-2,4,6-triiodo-benzoylamino]-propyl ester

Base Information

Chemical Name:Acetic acid 2-acetoxy-3-[3-(2-acetoxy-1-acetoxymethyl-ethylcarbamoyl)-5-diacetylamino-2,4,6-triiodo-benzoylamino]-propyl ester
CAS No.:1186058-05-8
Molecular Formula:C₂₆H₃₀I₃N₃O₁₂
Molecular Weight:957.251
Hs Code.:

Synonyms:Acetic acid 2-acetoxy-3-[3-(2-acetoxy-1-acetoxymethyl-ethylcarbamoyl)-5-diacetylamino-2,4,6-triiodo-benzoylamino]-propyl ester

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Chemical Property of Acetic acid 2-acetoxy-3-[3-(2-acetoxy-1-acetoxymethyl-ethylcarbamoyl)-5-diacetylamino-2,4,6-triiodo-benzoylamino]-propyl ester

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Technology Process of Acetic acid 2-acetoxy-3-[3-(2-acetoxy-1-acetoxymethyl-ethylcarbamoyl)-5-diacetylamino-2,4,6-triiodo-benzoylamino]-propyl ester

There total 2 articles about Acetic acid 2-acetoxy-3-[3-(2-acetoxy-1-acetoxymethyl-ethylcarbamoyl)-5-diacetylamino-2,4,6-triiodo-benzoylamino]-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1096689-22-3
5-amino-N₁-(1,3-dihydroxypropan-2-yl)-N₃-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide

: 108-24-7
acetic anhydride

: 64-19-7,77671-22-8
acetic acid

: 1186058-05-8
Acetic acid 2-acetoxy-3-[3-(2-acetoxy-1-acetoxymethyl-ethylcarbamoyl)-5-diacetylamino-2,4,6-triiodo-benzoylamino]-propyl ester

Guidance literature:: With NC₁₀₀₁₈₁; acetyl chloride; at 23 - 100 ℃; for 18h;

Reference yield:

: 1186058-05-8
Acetic acid 2-acetoxy-3-[3-(2-acetoxy-1-acetoxymethyl-ethylcarbamoyl)-5-diacetylamino-2,4,6-triiodo-benzoylamino]-propyl ester

Guidance literature:

Reference yield: 33.6%

: 1186058-05-8
Acetic acid 2-acetoxy-3-[3-(2-acetoxy-1-acetoxymethyl-ethylcarbamoyl)-5-diacetylamino-2,4,6-triiodo-benzoylamino]-propyl ester

: 564-00-1,1464-53-5,30031-64-2,30419-67-1,34897-03-5,298-18-0
1,2:3,4-Diepoxybutane

: 1186058-02-5
5,5'-(2,3-dihydroxybutane-1,4-diyl)bis(acetylazanediyl)bis(N₁-(1,3-dihydroxypropan-2-yl)-N₃-(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide)

Guidance literature:: Acetic acid 2-acetoxy-3-[3-(2-acetoxy-1-acetoxymethyl-ethylcarbamoyl)-5-diacetylamino-2,4,6-triiodo-benzoylamino]-propyl ester; With water; boric acid; potassium hydroxide; In methanol; at 10 - 14 ℃; for 31h; pH=12.5 - 12.8;

1,2:3,4-Diepoxybutane; In methanol; water; at 10 - 20 ℃; for 141h; pH=12.5 - 12.8;

With hydrogenchloride; In methanol; water; pH=1.2 - 7.5;