Technology Process of C42H41ClO5
There total 5 articles about C42H41ClO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Dess-Martin periodane;
In
dichloromethane;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 20 °C
2: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 1 h / 20 °C
3: Dess-Martin periodane / dichloromethane / 3 h / 20 °C
With
triethylsilane; boron trifluoride diethyl etherate; sodium hydride; Dess-Martin periodane;
In
dichloromethane; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 20 h / 20 °C
2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 20 °C
3: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 1 h / 20 °C
4: Dess-Martin periodane / dichloromethane / 3 h / 20 °C
With
triethylsilane; boron trifluoride diethyl etherate; sodium hydride; Dess-Martin periodane; toluene-4-sulfonic acid;
In
dichloromethane; N,N-dimethyl-formamide; mineral oil;