6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

Base Information

Chemical Name:6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine
CAS No.:1398564-48-1
Molecular Formula:C₁₇H₁₀Cl₂N₂O₂S₄
Molecular Weight:473.449
Hs Code.:

Synonyms:6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

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Chemical Property of 6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

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Technology Process of 6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

There total 3 articles about 6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1398564-99-2
6-chloro-3-methylthio-7-thiocarbamoyl-1,1-dioxo-1,4,2-benzodithiazine

: 536-38-9
4-chlorobenzoylmethyl bromide

: 1398564-48-1
6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

Guidance literature:: In methanol; Reflux;
DOI:10.1016/j.ejmech.2012.07.042

Reference yield:

: 156775-43-8
6-chloro-3-metylotio-1,1-diokso-1,4,2-benzoditiazyno-7-karboksyamid

: 1398564-48-1
6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

Guidance literature:: Multi-step reaction with 2 steps

1: Lawessons reagent / toluene / 1 h / 110 °C

2: methanol / Reflux

With Lawessons reagent; In methanol; toluene;
DOI:10.1016/j.ejmech.2012.07.042

Reference yield:

: 6-chloro-3-(methylthio)-1,1-dioxo-1,4,2-benzodithiazine-7-carboxylic acid

: 1398564-48-1
6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / benzene / Reflux

1.2: 5 - 10 °C

2.1: Lawessons reagent / toluene / 1 h / 110 °C

3.1: methanol / Reflux

With Lawessons reagent; thionyl chloride; In methanol; toluene; benzene;
DOI:10.1016/j.ejmech.2012.07.042