3-amino-6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-1,1-dioxo-1,4,2-benzodithiazine

Base Information

Chemical Name:3-amino-6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-1,1-dioxo-1,4,2-benzodithiazine
CAS No.:1398564-52-7
Molecular Formula:C₁₆H₉Cl₂N₃O₂S₃
Molecular Weight:442.37
Hs Code.:

Synonyms:3-amino-6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-1,1-dioxo-1,4,2-benzodithiazine

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Chemical Property of 3-amino-6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-1,1-dioxo-1,4,2-benzodithiazine

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Technology Process of 3-amino-6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-1,1-dioxo-1,4,2-benzodithiazine

There total 4 articles about 3-amino-6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-1,1-dioxo-1,4,2-benzodithiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1398564-48-1
6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

: 1398564-52-7
3-amino-6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-1,1-dioxo-1,4,2-benzodithiazine

Guidance literature:: With ammonium hydroxide; In methanol; at 0 - 20 ℃;
DOI:10.1016/j.ejmech.2012.07.042

Reference yield:

: 156775-43-8
6-chloro-3-metylotio-1,1-diokso-1,4,2-benzoditiazyno-7-karboksyamid

: 1398564-52-7
3-amino-6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-1,1-dioxo-1,4,2-benzodithiazine

Guidance literature:: Multi-step reaction with 3 steps

1: Lawessons reagent / toluene / 1 h / 110 °C

2: methanol / Reflux

3: ammonium hydroxide / methanol / 0 - 20 °C

With Lawessons reagent; ammonium hydroxide; In methanol; toluene;
DOI:10.1016/j.ejmech.2012.07.042

Reference yield:

: 6-chloro-3-(methylthio)-1,1-dioxo-1,4,2-benzodithiazine-7-carboxylic acid

: 1398564-52-7
3-amino-6-chloro-7-[4-(4-chlorophenyl)thiazol-2-yl]-1,1-dioxo-1,4,2-benzodithiazine

Guidance literature:: Multi-step reaction with 4 steps

1.1: thionyl chloride / benzene / Reflux

1.2: 5 - 10 °C

2.1: Lawessons reagent / toluene / 1 h / 110 °C

3.1: methanol / Reflux

4.1: ammonium hydroxide / methanol / 0 - 20 °C

With Lawessons reagent; ammonium hydroxide; thionyl chloride; In methanol; toluene; benzene;
DOI:10.1016/j.ejmech.2012.07.042