N-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenyl]-formamide

Base Information

Chemical Name:N-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenyl]-formamide
CAS No.:114772-29-1
Molecular Formula:C₁₇H₂₂ClN₃O₂
Molecular Weight:335.834
Hs Code.:

Synonyms:N-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenyl]-formamide

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Chemical Property of N-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenyl]-formamide

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Technology Process of N-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenyl]-formamide

There total 5 articles about N-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenyl]-formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114799-96-1
2-n-butyl-4-chloro-5-(methoxymethyl)-1-<(4-nitrophenyl)methyl>imidazole

: 114772-29-1
N-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenyl]-formamide

Guidance literature:: Multi-step reaction with 2 steps

1: 56.5 percent / H₂ / 10percent Pd/C / methanol / 4 h

2: 9.52 g / Heating

With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00167a007

Reference yield:

: 114799-92-7
2-Butyl-4-chloro-1-[(4-nitrophenyl)methyl]-1H-imidazole-5-methanol

: 114772-29-1
N-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenyl]-formamide

Guidance literature:: Multi-step reaction with 3 steps

1: 11.57 g / concd. sulfuric acid / Heating

2: 56.5 percent / H₂ / 10percent Pd/C / methanol / 4 h

3: 9.52 g / Heating

With sulfuric acid; hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00167a007

Reference yield:

: 79047-41-9
2-n-butyl-4-chloro-5-hydroxymethylimidazole

: 114772-29-1
N-[4-(2-Butyl-4-chloro-5-methoxymethyl-imidazol-1-ylmethyl)-phenyl]-formamide

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) sodium methoxide / 1.) methanol, 0 deg C, 2.) DMF, 25 deg C

2: 11.57 g / concd. sulfuric acid / Heating

3: 56.5 percent / H₂ / 10percent Pd/C / methanol / 4 h

4: 9.52 g / Heating

With sulfuric acid; hydrogen; sodium methylate; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00167a007