ethyl 5-(4-bromophenyl)-2,2,2-triphenyl-5-(trifluoromethyl)-2,5-dihydro-1,2λ⁵-oxaphosphole-4-carboxylate

Base Information

• Chemical Name: ethyl 5-(4-bromophenyl)-2,2,2-triphenyl-5-(trifluoromethyl)-2,5-dihydro-1,2λ⁵-oxaphosphole-4-carboxylate
• CAS No.: 1418009-88-7
• Molecular Formula: C₃₁H₂₅BrF₃O₃P
• Molecular Weight: 613.411

Synonyms:ethyl 5-(4-bromophenyl)-2,2,2-triphenyl-5-(trifluoromethyl)-2,5-dihydro-1,2λ⁵-oxaphosphole-4-carboxylate

Chemical Property of ethyl 5-(4-bromophenyl)-2,2,2-triphenyl-5-(trifluoromethyl)-2,5-dihydro-1,2λ⁵-oxaphosphole-4-carboxylate

Chemical Property:

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Technology Process of ethyl 5-(4-bromophenyl)-2,2,2-triphenyl-5-(trifluoromethyl)-2,5-dihydro-1,2λ⁵-oxaphosphole-4-carboxylate

There total 1 articles about ethyl 5-(4-bromophenyl)-2,2,2-triphenyl-5-(trifluoromethyl)-2,5-dihydro-1,2λ⁵-oxaphosphole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4'-bromo-2,2,2-trifluoroacetophenone (16184-89-7) + triphenylphosphine (603-35-0) + propynoic acid ethyl ester (623-47-2) → ethyl 5-(4-bromophenyl)-2,2,2-triphenyl-5-(trifluoromethyl)-2,5-dihydro-1,2λ5-oxaphosphole-4-carboxylate (1418009-88-7)

Guidance literature:

In ethyl acetate; at 20 ℃; for 8h;

DOI:10.1055/s-0032-1316799

upstream raw materials:

4'-bromo-2,2,2-trifluoroacetophenone

triphenylphosphine

propynoic acid ethyl ester

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