(+/-)-cis-2-butyl-5-heptylpyrrolidine

Base Information

Chemical Name:(+/-)-cis-2-butyl-5-heptylpyrrolidine
CAS No.:116558-83-9
Molecular Formula:C₁₅H₃₁N
Molecular Weight:225.418
Hs Code.:

Synonyms:(+/-)-cis-2-butyl-5-heptylpyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-cis-2-butyl-5-heptylpyrrolidine

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Technology Process of (+/-)-cis-2-butyl-5-heptylpyrrolidine

There total 16 articles about (+/-)-cis-2-butyl-5-heptylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1258206-78-8
8-azidopentadecan-5-one

: 116558-84-0,71732-80-4
(+/-)-trans-2-butyl-5-heptylpyrrolidine

: 116558-83-9,71732-80-4
(+/-)-cis-2-butyl-5-heptylpyrrolidine

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 24h; optical yield given as %de;
DOI:10.1021/ja1068036

Reference yield: 63.0%

: Methanesulfonic acid 1-[(2R,5S)-1-methanesulfonyl-5-(2-methanesulfonyloxy-butyl)-pyrrolidin-2-ylmethyl]-hexyl ester

: 116558-83-9,71732-80-4
(+/-)-cis-2-butyl-5-heptylpyrrolidine

Guidance literature:: Methanesulfonic acid 1-[(2R,5S)-1-methanesulfonyl-5-(2-methanesulfonyloxy-butyl)-pyrrolidin-2-ylmethyl]-hexyl ester; With lithium triethylborohydride;

With sodium bis(2-methoxyethoxy)aluminium dihydride;
DOI:10.7164/antibiotics.53.467

Reference yield:

: 18356-28-0
tetrahydro-pyrrolizin-3,5-dione

: 116558-83-9,71732-80-4
(+/-)-cis-2-butyl-5-heptylpyrrolidine

Guidance literature:: Multi-step reaction with 7 steps

1: 89 percent / CH₂Cl₂ / Ambient temperature

2: 84 percent / BF₃*Et₂O / Ambient temperature

3: 87 percent / H₂ / Raney Ni / ethanol / 20 h / Heating

4: 75 percent / P₂S₅ / benzene / 1 h / Heating

5: 93 percent / CH₂Cl₂ / Ambient temperature

6: 29 percent / CH₂Cl₂ / 48 h / Heating

7: NaBH₄ / methanol / 0.5 h / Ambient temperature

With sodium tetrahydroborate; tetraphosphorus decasulfide; boron trifluoride diethyl etherate; hydrogen; nickel; In methanol; ethanol; dichloromethane; benzene;
DOI:10.1002/hlca.19870700805