(2R,5S)-2-butyl-5-heptyl-1-[(4-methylphenyl)sulfonyl]pyrrolidine

Base Information

Chemical Name:(2R,5S)-2-butyl-5-heptyl-1-[(4-methylphenyl)sulfonyl]pyrrolidine
CAS No.:123994-01-4
Molecular Formula:C22H37 N O2 S
Molecular Weight:379.5997
Hs Code.:
Mol file:123994-01-4.mol

Synonyms:Pyrrolidine,2-butyl-5-heptyl-1-[(4-methylphenyl)sulfonyl]-, cis- (9CI); Pyrrolidine,2-butyl-5-heptyl-1-[(4-methylphenyl)sulfonyl]-, cis-(?à)-

Suppliers and Price of (2R,5S)-2-butyl-5-heptyl-1-[(4-methylphenyl)sulfonyl]pyrrolidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of (2R,5S)-2-butyl-5-heptyl-1-[(4-methylphenyl)sulfonyl]pyrrolidine

Chemical Property:

Vapor Pressure:1.59E-09mmHg at 25°C
Boiling Point:484.1°C at 760 mmHg
Flash Point:246.6°C
Density:1.014g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2R,5S)-2-butyl-5-heptyl-1-[(4-methylphenyl)sulfonyl]pyrrolidine

There total 14 articles about (2R,5S)-2-butyl-5-heptyl-1-[(4-methylphenyl)sulfonyl]pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1310050-87-3
1-[5-butyl-1-(p-toluenesulfonyl)pyrrol-2-yl]heptan-1-one

: 123993-98-6
trans-N-(p-tolylsulfonyl)-2-heptyl-5-butylpyrrolidine

: 123994-01-4
cis-N-(p-tolylsulfonyl)-2-heptyl-5-butylpyrrolidine

Guidance literature:: 1-[5-butyl-1-(p-toluenesulfonyl)pyrrol-2-yl]heptan-1-one; With sodium cyanoborohydride; In dichloromethane; trifluoroacetic acid; at 0 - 20 ℃;

With palladium 10% on activated carbon; hydrogen; In methanol; for 3.5h; under 2068.65 Torr;
DOI:10.1039/c1ob05111c

Reference yield:

: 1310050-87-3
1-[5-butyl-1-(p-toluenesulfonyl)pyrrol-2-yl]heptan-1-one

: cis-2-butyl-5-heptyl-1-(p-toluenesulfonyl)-2,5-dihydropyrrole

: 123994-01-4
cis-N-(p-tolylsulfonyl)-2-heptyl-5-butylpyrrolidine

Guidance literature:: With sodium cyanoborohydride; In dichloromethane; trifluoroacetic acid; at 0 - 20 ℃;
DOI:10.1039/c1ob05111c

Reference yield:

: 1310050-85-1
2-butyl-1-(p-toluenesulfonyl)pyrrole

: cis-2-butyl-5-heptyl-1-(p-toluenesulfonyl)-2,5-dihydropyrrole

: 123994-01-4
cis-N-(p-tolylsulfonyl)-2-heptyl-5-butylpyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane; trifluoroacetic anhydride / 20 °C

2: sodium cyanoborohydride / dichloromethane; trifluoroacetic acid / 0 - 20 °C

With sodium cyanoborohydride; In dichloromethane; trifluoroacetic acid; trifluoroacetic anhydride;
DOI:10.1039/c1ob05111c