Phosphorous triamide,N,N',N''-triphenyl- (8CI,9CI)

Base Information

• Chemical Name: Phosphorous triamide,N,N',N''-triphenyl- (8CI,9CI)
• CAS No.: 15159-51-0
• Molecular Formula: C18H18 N3 P
• Molecular Weight: 307.335
• Mol file: 15159-51-0.mol

Synonyms:Phosphorousacid trianilide; Phosphorous acid triphenylamide; Phosphorous trianilide;Phosphorustrianilide; Tris(phenylamido) phosphite

Chemical Property of Phosphorous triamide,N,N',N''-triphenyl- (8CI,9CI)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phosphorous triamide,N,N',N''-triphenyl- (8CI,9CI)

There total 3 articles about Phosphorous triamide,N,N',N''-triphenyl- (8CI,9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.5%

N,N,N’,N’-tetraethyl-P-phenyl-phosphonic diamide (4519-35-1) + aniline (62-53-3) → triphenyl phosphite (101-02-0) + N,N',N''-triphenylphosphorous triamide (15159-51-0) + phenyl N,N'-diphenylphosphorodiamidite (26350-11-8) + diphenyl phenylphosphoramidite (26350-10-7) + diethylamine (109-89-7)

Guidance literature:

for 17h; Product distribution; Heating;

Reference yield: 68.0%

aniline (62-53-3) → N,N',N''-triphenylphosphorous triamide (15159-51-0)

Guidance literature:

With hexaethylphosphoric triamide; at 60 - 65 ℃; for 8h;

Reference yield:

→ N,N',N''-triphenylphosphorous triamide (15159-51-0)

Guidance literature:

/BRN= 715371/, Anilin;

upstream raw materials:

N,N,N’,N’-tetraethyl-P-phenyl-phosphonic diamide

aniline

Downstream raw materials:

Mo(CO)4(P(C₆H₅NH)2)2NC₆H₅*0.5C₆H₆

bis(anilino)phosphine oxide

N-phenyl benzoyl amide

Refernces

• 1、 Feshchenko, N. G.,Rutkovskii, E. K.,Gorbatenko, Zh. K.. "REACTION OF PHOSPHORUS AND IODINE". . p. 1498 - 1499. Retrieved 2007/10/02.
• 2、 Trishin, Yu. G.,Chistokletov, V. N.. "REACTIONS OF N,N,N',N'-TETRAETHYL-P-PHENYLPHOSPHONOUS DIAMIDE AND OF PHENYL TETRAETHYLPHOSPHORODIAMIDITE WITH PRIMARY AROMATIC AMINES". . p. 2188 - 2191. Retrieved 2007/10/02.