tert-butyl 3-oxo-4-(phenylsulfinyl)-2-(triphenylphosphoranylidene)butanoate

Base Information

Chemical Name:tert-butyl 3-oxo-4-(phenylsulfinyl)-2-(triphenylphosphoranylidene)butanoate
CAS No.:1352703-53-7
Molecular Formula:C₃₂H₃₁O₄PS
Molecular Weight:542.635
Hs Code.:

Synonyms:tert-butyl 3-oxo-4-(phenylsulfinyl)-2-(triphenylphosphoranylidene)butanoate

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Chemical Property of tert-butyl 3-oxo-4-(phenylsulfinyl)-2-(triphenylphosphoranylidene)butanoate

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Technology Process of tert-butyl 3-oxo-4-(phenylsulfinyl)-2-(triphenylphosphoranylidene)butanoate

There total 1 articles about tert-butyl 3-oxo-4-(phenylsulfinyl)-2-(triphenylphosphoranylidene)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 86302-43-4,35000-38-5
(tert-Butoxycarbonylmethylene)triphenylphosphorane

: 3959-08-8,60833-02-5,60833-03-6,90693-85-9
(phenylsulfinyl)acetic acid

: 1352703-53-7
tert-butyl 3-oxo-4-(phenylsulfinyl)-2-(triphenylphosphoranylidene)butanoate

Guidance literature:: With dmap; 1,2-dichloro-ethane; In dichloromethane; at 0 - 20 ℃; for 13h; Inert atmosphere;
DOI:10.5012/bkcs.2011.32.9.3477

Reference yield:

: 629-27-6
1-Iodooctane

: 1352703-53-7
tert-butyl 3-oxo-4-(phenylsulfinyl)-2-(triphenylphosphoranylidene)butanoate

: C₃₅H₃₈BrO₂PS

Guidance literature:: tert-butyl 3-oxo-4-(phenylsulfinyl)-2-(triphenylphosphoranylidene)butanoate; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.333333h; Inert atmosphere;

1-Iodooctane; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.5012/bkcs.2011.32.9.3477

Reference yield:

: 4119-41-9
1-iodo-3-phenylpropan

: 1352703-53-7
tert-butyl 3-oxo-4-(phenylsulfinyl)-2-(triphenylphosphoranylidene)butanoate

: C₃₆H₃₂BrO₂PS

Guidance literature:: tert-butyl 3-oxo-4-(phenylsulfinyl)-2-(triphenylphosphoranylidene)butanoate; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.333333h; Inert atmosphere;

1-iodo-3-phenylpropan; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.5012/bkcs.2011.32.9.3477