1-IODO-3-PHENYLPROPANE

Base Information

• Chemical Name: 1-IODO-3-PHENYLPROPANE
• CAS No.: 4119-41-9
• Molecular Formula: C9H11 I
• Molecular Weight: 246.091
• Hs Code.: 2903999090
• Mol file: 4119-41-9.mol

Synonyms:(3-Iodopropyl)benzene;1-Iodo-3-phenylpropane; 3-Iodo-1-phenylpropane; 3-Phenyl-1-iodopropane;3-Phenylpropyl iodide

Chemical Property of 1-IODO-3-PHENYLPROPANE

Chemical Property:

• Vapor Pressure: 0.0391mmHg at 25°C
• Melting Point: 54-56 °C(Solv: ethyl acetate (141-78-6); ethyl ether (60-29-7))
• Refractive Index: n20/D 1.5820(lit.)
• Boiling Point: 248°Cat760mmHg
• Flash Point: 104.9°C
• PSA: 0.00000
• Density: 1.561g/cm³
• LogP: 3.05420
• Sensitive.: Light Sensitive

Purity/Quality:

98%,99%, ^*data from raw suppliers

1-Iodo-3-phenylpropane 97% ^*data from reagent suppliers

Safty Information:

• Safety Statements: S24/25:Avoid contact with skin and eyes.

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 1-IODO-3-PHENYLPROPANE

There total 49 articles about 1-IODO-3-PHENYLPROPANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-phenylpropyl 4-methylbenzenesulfonate (3742-75-4) → 1-iodo-3-phenylpropan (4119-41-9)

Guidance literature:

With sodium iodide; In acetone;

DOI:10.1016/j.tetasy.2005.09.009

Reference yield: 100.0%

3-methoxypropylbenzene (2046-33-5) → 1-iodo-3-phenylpropan (4119-41-9)

Guidance literature:

With sodium iodide; In N,N-dimethyl acetamide; at 100 ℃; for 12h; Temperature;

DOI:10.1039/c9sc03347e

Reference yield: 100.0%

1-Phenyl-1-propanol (93-54-9) + ethyl iodide (75-03-6) → (±)-(1-iodopropyl)benzene (4119-41-9)

Guidance literature:

ethyl iodide; With magnesium; N-butylpyridinium tetrafluoroborate; at 20 ℃; for 1h;

1-Phenyl-1-propanol; With magnesium iodide; at 20 ℃; for 12h; Further stages.;

DOI:10.1039/b602718k

upstream raw materials:

3-Phenyl-1-propanol

phenylpropyl chloride

methyl iodide

Chloroiodomethane

Downstream raw materials:

N-ethyl-N-(3-phenylpropyl)aniline

2-(4-phenyl-butyl)-4,5-dihydro-thiazole

2-(1-chloro-4-phenyl-butyl)-4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazine

(hexa-4,5-dien-1-yl)benzene

Refernces

• 1、 Bekere, Laura,Lokshin, Vladimir,Sigalov, Mark,Gvishi, Raz,Zhao, Peng,Hagan, David J.,Van Stryland, Eric W.,Khodorkovsky, Vladimir. "Chromenes involving a two-photon absorbing moiety: Photochromism via intramolecular resonance energy transfer". . p. 1143 - 1148. Retrieved 2016.
• 2、 Epifanov, Maxim,Mo, Jia Yi,Dubois, Rudy,Yu, Hao,Sammis, Glenn M.. "One-Pot Deoxygenation and Substitution of Alcohols Mediated by Sulfuryl Fluoride". . p. 3768 - 3777. Retrieved 2021/03/01.
• 3、 Dussault, Patrick H.,Horn, Alissa. "A click-based modular approach to introduction of peroxides onto molecules and nanostructures". . p. 44408 - 44429. Retrieved 2020/12/28.