3-Hydroxy-2-[1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-oxo-2-phenylethyl]-5,5-dimethylcyclohex-2-en-1-on

Base Information

• Chemical Name: 3-Hydroxy-2-[1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-oxo-2-phenylethyl]-5,5-dimethylcyclohex-2-en-1-on
• CAS No.: 123271-58-9
• Molecular Formula: C₂₄H₂₈O₅
• Molecular Weight: 396.483

Synonyms:3-Hydroxy-2-[1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-oxo-2-phenylethyl]-5,5-dimethylcyclohex-2-en-1-on

Chemical Property of 3-Hydroxy-2-[1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-oxo-2-phenylethyl]-5,5-dimethylcyclohex-2-en-1-on

Chemical Property:

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Technology Process of 3-Hydroxy-2-[1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-oxo-2-phenylethyl]-5,5-dimethylcyclohex-2-en-1-on

There total 2 articles about 3-Hydroxy-2-[1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-oxo-2-phenylethyl]-5,5-dimethylcyclohex-2-en-1-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

phenylglyoxal hydrate (1074-12-0) + dimedone (126-81-8) → 3-Hydroxy-2-[1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-oxo-2-phenylethyl]-5,5-dimethylcyclohex-2-en-1-on (123271-58-9)

Guidance literature:

In ethanol; water; Heating;

DOI:10.1002/hlca.200490085

Reference yield:

dimedone (126-81-8) + C23H15N3O4 → 3-Hydroxy-2-[1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-oxo-2-phenylethyl]-5,5-dimethylcyclohex-2-en-1-on (123271-58-9)

Guidance literature:

With triethylamine; Yield given. Multistep reaction; 1.) THF, 0 deg C, 25 min, 2.) THF, RT, 12 h;

Reference yield: 45.0%

6-amino-2-methylsulfanylpyrimidin-4(3H)-one (1074-41-5) + 3-Hydroxy-2-[1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-oxo-2-phenylethyl]-5,5-dimethylcyclohex-2-en-1-on (123271-58-9) → 5-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)-2-(methylsulfanyl)-6-phenyl-3,7-dihydro-4H-pyrrolo[2,3-d]-pyrimidin-4-one (1253375-32-4)

Guidance literature:

With acetic acid; In ethanol; for 9h; Heating;

DOI:10.1016/j.tetlet.2010.08.021

upstream raw materials:

phenylglyoxal hydrate

dimedone

Downstream raw materials:

3-(2-Hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-1-isobutyl-6,6-dimethyl-2-phenyl-1,5,6,7-tetrahydro-indol-4-one

3-(2-Hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-6,6-dimethyl-1,2-diphenyl-1,5,6,7-tetrahydro-indol-4-one

13-Benzoyl-3,3,10,10-tetramethyldispiro[5.0.5.1]tridecan-1,5,8,12-tetron

C₂₀H₂₁N₅O₂

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